# Electronic Supplementary Material (ESI) for Chemical Communications. # This journal is © The Royal Society of Chemistry 2023 ####################################################################### # # This file contains crystal structure data downloaded from the # Cambridge Structural Database (CSD) hosted by the Cambridge # Crystallographic Data Centre (CCDC). # # Full information about CCDC data access policies and citation # guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 # # Audit and citation data items may have been added by the CCDC. # Please retain this information to preserve the provenance of # this file and to allow appropriate attribution of the data. # ####################################################################### data_av098 _database_code_depnum_ccdc_archive 'CCDC 2254388' loop_ _audit_author_name _audit_author_address 'Peter Mayer' ;LMU Muenchen Germany ; _audit_update_record ; 2023-04-06 deposited with the CCDC. 2023-05-10 downloaded from the CCDC. ; _chemical_name_common unknowncrystal _chemical_compound_source ? _chemical_absolute_configuration ? _exptl_crystal_description platelet _exptl_crystal_colour colourless _exptl_crystal_size_max 0.150 #?# in millimeters _exptl_crystal_size_mid 0.130 #?# in millimeters _exptl_crystal_size_min 0.040 #?# in millimeters _exptl_crystal_density_method 'not measured' _exptl_crystal_density_meas ? _exptl_special_details ; ; _audit_creation_date ? #?# style: 18-Aug-1998 _diffrn_ambient_temperature 173.(2) #?# in K _diffrn_source_type 'Bruker TXS' _diffrn_source_power 2.5 #?# in kW _diffrn_source_voltage 50 #?# in kV _diffrn_source_current 50 #?# in mA _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'rotating anode (TXS)' _diffrn_radiation_monochromator 'focusing mirrors' _diffrn_radiation_collimation ? _diffrn_measurement_device 'fixed-chi three-circle diffractometer' _diffrn_measurement_device_type 'Bruker D8 Venture TXS' _diffrn_measurement_method 'mix of phi and omega scans' _diffrn_measurement_details ? _diffrn_detector_area_resol_mean 7.3910 _diffrn_special_details ? _diffrn_orient_matrix_type ? _diffrn_orient_matrix_UB_11 ? _diffrn_orient_matrix_UB_12 ? _diffrn_orient_matrix_UB_13 ? _diffrn_orient_matrix_UB_21 ? _diffrn_orient_matrix_UB_22 ? _diffrn_orient_matrix_UB_23 ? _diffrn_orient_matrix_UB_31 ? _diffrn_orient_matrix_UB_32 ? _diffrn_orient_matrix_UB_33 ? _cell_length_a 18.5673(6) _cell_length_b 5.8814(2) _cell_length_c 15.1443(6) _cell_angle_alpha 90 _cell_angle_beta 99.7200(10) _cell_angle_gamma 90 _cell_volume 1630.04(10) _cell_measurement_temperature 173.(2) #?# in K _cell_measurement_reflns_used 9875 _cell_measurement_theta_min 2.7291 _cell_measurement_theta_max 27.4914 _cell_special_details ? _exptl_absorpt_coefficient_mu 0.196 _exptl_absorpt_correction_type Multi-Scan _exptl_absorpt_correction_T_min 0.95 _exptl_absorpt_correction_T_max 0.99 _shelx_estimated_absorpt_T_min 0.971 _shelx_estimated_absorpt_T_max 0.992 _exptl_absorpt_process_details ; SADABS-2016/2 - Bruker AXS area detector scaling and absorption correction ; _diffrn_reflns_number 27725 #xl _diffrn_reflns_av_R_equivalents 0.0415 #xl _diffrn_reflns_av_unetI/netI 0.0257 #xl _diffrn_reflns_limit_h_min -24 #xl _diffrn_reflns_limit_h_max 24 #xl _diffrn_reflns_limit_k_min -7 #xl _diffrn_reflns_limit_k_max 7 #xl _diffrn_reflns_limit_l_min -19 #xl _diffrn_reflns_limit_l_max 19 #xl _diffrn_reflns_theta_min 3.117 #xl _diffrn_reflns_theta_max 27.482 #xl _diffrn_measured_fraction_theta_max 0.999 #xl _diffrn_reflns_theta_full 25.242 #xl _diffrn_measured_fraction_theta_full 0.998 #xl _diffrn_reflns_Laue_measured_fraction_max 0.999 #xl _diffrn_reflns_Laue_measured_fraction_full 0.998 #xl _diffrn_reflns_point_group_measured_fraction_max 0.999 #xl _diffrn_reflns_point_group_measured_fraction_full 0.998 #xl _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'P 1 21/c 1' _space_group_name_Hall '-P 2ybc' _space_group_IT_number 14 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _reflns_number_total 3740 #xl _reflns_number_gt 3312 #xl _reflns_threshold_expression 'I > 2\s(I)' #xl _reflns_Friedel_coverage 0.000 #xl _reflns_Friedel_fraction_max . #xl _reflns_Friedel_fraction_full . #xl _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _refine_ls_structure_factor_coef Fsqd #xl _refine_ls_matrix_type full #xl _refine_ls_weighting_scheme calc #xl _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0347P)^2^+0.7093P] where P=(Fo^2^+2Fc^2^)/3' #xl _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment constr #?# _refine_ls_extinction_method none #xl _refine_ls_extinction_coef . #xl _refine_ls_abs_structure_details ? #xl _refine_ls_abs_structure_Flack ? #xl _refine_ls_number_reflns 3740 #xl _refine_ls_number_parameters 194 #xl _refine_ls_number_restraints 0 #xl _refine_ls_R_factor_all 0.0419 #xl _refine_ls_R_factor_gt 0.0359 #xl _refine_ls_wR_factor_ref 0.0924 #xl _refine_ls_wR_factor_gt 0.0892 #xl _refine_ls_goodness_of_fit_ref 1.104 #xl _refine_ls_restrained_S_all 1.104 #xl _refine_ls_shift/su_max 0.001 #xl _refine_ls_shift/su_mean 0.000 #xl _refine_diff_density_max 0.276 #xl _refine_diff_density_min -0.217 #xl _refine_diff_density_rms 0.041 #xl _refine_special_details ; ; _computing_data_collection 'APEX3 v2016.5-0, Bruker AXS (2016)' _computing_cell_refinement 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_data_reduction 'SAINT V8.38A (Bruker AXS Inc., 2017)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 924)' _computing_publication_material ? loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.03487(8) 0.0884(3) 0.65177(10) 0.0331(3) Uani 1 1 d . . . . . C2 C 0.05962(8) -0.1412(3) 0.63556(10) 0.0303(3) Uani 1 1 d . . . . . H2A H 0.043277 -0.182001 0.571906 0.036 Uiso 1 1 calc R U . . . H2AB H 0.037630 -0.250829 0.672910 0.036 Uiso 1 1 calc R U . . . C3 C 0.18011(7) 0.0024(2) 0.57245(8) 0.0217(3) Uani 1 1 d . . . . . C4 C 0.25849(7) 0.0779(2) 0.57424(8) 0.0207(3) Uani 1 1 d . . . . . C5 C 0.16964(7) 0.2046(2) 0.44617(9) 0.0224(3) Uani 1 1 d . . . . . C6 C 0.30398(7) 0.3070(2) 0.45875(9) 0.0227(3) Uani 1 1 d . . . . . H6 H 0.351215 0.274933 0.491386 0.027 Uiso 1 1 calc R U . . . C7 C 0.30215(7) 0.4586(2) 0.39209(9) 0.0242(3) Uani 1 1 d . . . . . H7 H 0.256296 0.493158 0.356432 0.029 Uiso 1 1 calc R U . . . C8 C 0.36742(7) 0.5733(2) 0.37174(8) 0.0231(3) Uani 1 1 d . . . . . C9 C 0.43779(7) 0.4824(3) 0.39295(9) 0.0273(3) Uani 1 1 d . . . . . H9 H 0.444450 0.337231 0.420661 0.033 Uiso 1 1 calc R U . . . C10 C 0.49801(8) 0.6006(3) 0.37418(10) 0.0333(3) Uani 1 1 d . . . . . H10 H 0.545382 0.536108 0.389552 0.040 Uiso 1 1 calc R U . . . C11 C 0.48985(8) 0.8113(3) 0.33334(10) 0.0344(3) Uani 1 1 d . . . . . H11 H 0.531253 0.891648 0.320523 0.041 Uiso 1 1 calc R U . . . C12 C 0.42062(9) 0.9037(3) 0.31135(10) 0.0336(3) Uani 1 1 d . . . . . H12 H 0.414424 1.048238 0.283113 0.040 Uiso 1 1 calc R U . . . C13 C 0.36025(8) 0.7865(3) 0.33026(9) 0.0287(3) Uani 1 1 d . . . . . H13 H 0.313087 0.852377 0.314749 0.034 Uiso 1 1 calc R U . . . C14 C 0.28254(8) 0.2439(2) 0.65152(9) 0.0276(3) Uani 1 1 d . . . . . H14A H 0.329660 0.311336 0.645193 0.041 Uiso 1 1 calc R U . . . H14B H 0.287438 0.162164 0.708614 0.041 Uiso 1 1 calc R U . . . H14C H 0.245903 0.364333 0.650187 0.041 Uiso 1 1 calc R U . . . C15 C 0.31109(8) -0.1232(2) 0.57827(10) 0.0296(3) Uani 1 1 d . . . . . H15A H 0.359282 -0.068702 0.569575 0.044 Uiso 1 1 calc R U . . . H15B H 0.292477 -0.232294 0.530985 0.044 Uiso 1 1 calc R U . . . H15C H 0.315244 -0.197516 0.636827 0.044 Uiso 1 1 calc R U . . . C16 C 0.15689(8) 0.0989(3) 0.35264(9) 0.0313(3) Uani 1 1 d . . . . . H16A H 0.174328 -0.058668 0.356377 0.047 Uiso 1 1 calc R U . . . H16B H 0.183602 0.186025 0.313456 0.047 Uiso 1 1 calc R U . . . H16C H 0.104554 0.101453 0.328131 0.047 Uiso 1 1 calc R U . . . C17 C 0.13749(8) 0.4432(3) 0.44685(11) 0.0340(3) Uani 1 1 d . . . . . H17A H 0.150259 0.508499 0.506995 0.051 Uiso 1 1 calc R U . . . H17B H 0.084210 0.435202 0.430189 0.051 Uiso 1 1 calc R U . . . H17C H 0.157365 0.539105 0.403816 0.051 Uiso 1 1 calc R U . . . N1 N 0.01703(8) 0.2686(3) 0.66648(11) 0.0476(4) Uani 1 1 d . . . . . N2 N 0.13320(6) 0.06403(19) 0.50611(7) 0.0235(2) Uani 1 1 d . . . . . N3 N 0.24774(6) 0.1917(2) 0.48658(7) 0.0237(2) Uani 1 1 d . . . . . S1 S 0.15850(2) -0.15927(6) 0.66218(2) 0.02729(10) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0253(7) 0.0424(9) 0.0319(8) -0.0006(7) 0.0060(6) -0.0023(6) C2 0.0282(7) 0.0320(7) 0.0332(8) 0.0017(6) 0.0120(6) -0.0083(6) C3 0.0257(6) 0.0197(6) 0.0214(6) -0.0011(5) 0.0086(5) -0.0024(5) C4 0.0215(6) 0.0219(6) 0.0188(6) 0.0022(5) 0.0041(5) -0.0015(5) C5 0.0200(6) 0.0252(6) 0.0219(6) 0.0028(5) 0.0031(5) -0.0041(5) C6 0.0204(6) 0.0271(7) 0.0211(6) -0.0026(5) 0.0049(5) -0.0039(5) C7 0.0221(6) 0.0282(7) 0.0224(6) -0.0003(5) 0.0041(5) -0.0035(5) C8 0.0266(6) 0.0265(7) 0.0169(6) -0.0031(5) 0.0061(5) -0.0057(5) C9 0.0290(7) 0.0294(7) 0.0246(7) 0.0019(6) 0.0074(5) -0.0012(6) C10 0.0253(7) 0.0454(9) 0.0295(7) 0.0014(7) 0.0054(6) -0.0036(6) C11 0.0316(7) 0.0430(9) 0.0293(7) 0.0010(6) 0.0073(6) -0.0143(7) C12 0.0406(8) 0.0303(8) 0.0302(7) 0.0048(6) 0.0068(6) -0.0093(6) C13 0.0293(7) 0.0304(7) 0.0264(7) 0.0030(6) 0.0050(5) -0.0024(6) C14 0.0328(7) 0.0277(7) 0.0222(6) -0.0022(6) 0.0044(5) -0.0058(6) C15 0.0279(7) 0.0275(7) 0.0343(8) 0.0023(6) 0.0074(6) 0.0033(6) C16 0.0317(7) 0.0400(8) 0.0216(7) -0.0015(6) 0.0026(5) -0.0118(6) C17 0.0287(7) 0.0283(7) 0.0461(9) 0.0070(7) 0.0099(6) 0.0021(6) N1 0.0379(8) 0.0488(9) 0.0545(9) -0.0070(7) 0.0033(7) 0.0078(7) N2 0.0234(5) 0.0253(6) 0.0226(5) 0.0008(5) 0.0062(4) -0.0048(5) N3 0.0189(5) 0.0311(6) 0.0209(5) 0.0062(5) 0.0026(4) -0.0036(4) S1 0.02950(18) 0.02814(19) 0.02604(18) 0.00628(14) 0.00992(13) -0.00131(14) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 N1 1.144(2) . ? C1 C2 1.460(2) . ? C2 S1 1.8151(15) . ? C2 H2A 0.9900 . ? C2 H2AB 0.9900 . ? C3 N2 1.2664(17) . ? C3 C4 1.5174(17) . ? C3 S1 1.7595(13) . ? C4 N3 1.4699(16) . ? C4 C15 1.5285(19) . ? C4 C14 1.5314(18) . ? C5 N2 1.4741(16) . ? C5 N3 1.4776(16) . ? C5 C17 1.525(2) . ? C5 C16 1.5284(19) . ? C6 C7 1.3433(19) . ? C6 N3 1.3698(16) . ? C6 H6 0.9500 . ? C7 C8 1.4645(18) . ? C7 H7 0.9500 . ? C8 C9 1.3982(19) . ? C8 C13 1.399(2) . ? C9 C10 1.386(2) . ? C9 H9 0.9500 . ? C10 C11 1.382(2) . ? C10 H10 0.9500 . ? C11 C12 1.383(2) . ? C11 H11 0.9500 . ? C12 C13 1.386(2) . ? C12 H12 0.9500 . ? C13 H13 0.9500 . ? C14 H14A 0.9800 . ? C14 H14B 0.9800 . ? C14 H14C 0.9800 . ? C15 H15A 0.9800 . ? C15 H15B 0.9800 . ? C15 H15C 0.9800 . ? C16 H16A 0.9800 . ? C16 H16B 0.9800 . ? C16 H16C 0.9800 . ? C17 H17A 0.9800 . ? C17 H17B 0.9800 . ? C17 H17C 0.9800 . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N1 C1 C2 178.08(18) . . ? C1 C2 S1 110.60(10) . . ? C1 C2 H2A 109.5 . . ? S1 C2 H2A 109.5 . . ? C1 C2 H2AB 109.5 . . ? S1 C2 H2AB 109.5 . . ? H2A C2 H2AB 108.1 . . ? N2 C3 C4 117.36(11) . . ? N2 C3 S1 123.46(10) . . ? C4 C3 S1 119.17(9) . . ? N3 C4 C3 97.67(9) . . ? N3 C4 C15 112.13(11) . . ? C3 C4 C15 112.26(11) . . ? N3 C4 C14 112.18(11) . . ? C3 C4 C14 110.80(11) . . ? C15 C4 C14 111.15(11) . . ? N2 C5 N3 103.67(10) . . ? N2 C5 C17 106.92(11) . . ? N3 C5 C17 113.72(11) . . ? N2 C5 C16 109.09(11) . . ? N3 C5 C16 110.52(11) . . ? C17 C5 C16 112.40(12) . . ? C7 C6 N3 129.49(12) . . ? C7 C6 H6 115.3 . . ? N3 C6 H6 115.3 . . ? C6 C7 C8 123.18(12) . . ? C6 C7 H7 118.4 . . ? C8 C7 H7 118.4 . . ? C9 C8 C13 117.42(12) . . ? C9 C8 C7 123.36(13) . . ? C13 C8 C7 119.22(12) . . ? C10 C9 C8 121.05(14) . . ? C10 C9 H9 119.5 . . ? C8 C9 H9 119.5 . . ? C11 C10 C9 120.68(14) . . ? C11 C10 H10 119.7 . . ? C9 C10 H10 119.7 . . ? C10 C11 C12 119.16(14) . . ? C10 C11 H11 120.4 . . ? C12 C11 H11 120.4 . . ? C11 C12 C13 120.40(14) . . ? C11 C12 H12 119.8 . . ? C13 C12 H12 119.8 . . ? C12 C13 C8 121.29(14) . . ? C12 C13 H13 119.4 . . ? C8 C13 H13 119.4 . . ? C4 C14 H14A 109.5 . . ? C4 C14 H14B 109.5 . . ? H14A C14 H14B 109.5 . . ? C4 C14 H14C 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C4 C15 H15A 109.5 . . ? C4 C15 H15B 109.5 . . ? H15A C15 H15B 109.5 . . ? C4 C15 H15C 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? C5 C16 H16A 109.5 . . ? C5 C16 H16B 109.5 . . ? H16A C16 H16B 109.5 . . ? C5 C16 H16C 109.5 . . ? H16A C16 H16C 109.5 . . ? H16B C16 H16C 109.5 . . ? C5 C17 H17A 109.5 . . ? C5 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C5 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C3 N2 C5 108.87(11) . . ? C6 N3 C4 120.59(10) . . ? C6 N3 C5 126.36(11) . . ? C4 N3 C5 111.82(10) . . ? C3 S1 C2 98.68(6) . . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag N2 C3 C4 N3 -3.64(15) . . . . ? S1 C3 C4 N3 177.60(9) . . . . ? N2 C3 C4 C15 -121.40(13) . . . . ? S1 C3 C4 C15 59.83(14) . . . . ? N2 C3 C4 C14 113.67(13) . . . . ? S1 C3 C4 C14 -65.10(13) . . . . ? N3 C6 C7 C8 178.29(13) . . . . ? C6 C7 C8 C9 25.4(2) . . . . ? C6 C7 C8 C13 -153.57(14) . . . . ? C13 C8 C9 C10 0.6(2) . . . . ? C7 C8 C9 C10 -178.38(13) . . . . ? C8 C9 C10 C11 -0.5(2) . . . . ? C9 C10 C11 C12 0.1(2) . . . . ? C10 C11 C12 C13 0.2(2) . . . . ? C11 C12 C13 C8 0.0(2) . . . . ? C9 C8 C13 C12 -0.3(2) . . . . ? C7 C8 C13 C12 178.67(13) . . . . ? C4 C3 N2 C5 -1.22(16) . . . . ? S1 C3 N2 C5 177.49(9) . . . . ? N3 C5 N2 C3 5.55(14) . . . . ? C17 C5 N2 C3 -114.90(12) . . . . ? C16 C5 N2 C3 123.32(12) . . . . ? C7 C6 N3 C4 -164.38(14) . . . . ? C7 C6 N3 C5 1.9(2) . . . . ? C3 C4 N3 C6 175.14(12) . . . . ? C15 C4 N3 C6 -67.00(16) . . . . ? C14 C4 N3 C6 58.91(16) . . . . ? C3 C4 N3 C5 7.05(13) . . . . ? C15 C4 N3 C5 124.91(12) . . . . ? C14 C4 N3 C5 -109.18(12) . . . . ? N2 C5 N3 C6 -175.40(12) . . . . ? C17 C5 N3 C6 -59.68(18) . . . . ? C16 C5 N3 C6 67.83(17) . . . . ? N2 C5 N3 C4 -8.15(14) . . . . ? C17 C5 N3 C4 107.58(13) . . . . ? C16 C5 N3 C4 -124.92(12) . . . . ? N2 C3 S1 C2 -10.66(13) . . . . ? C4 C3 S1 C2 168.03(10) . . . . ? C1 C2 S1 C3 -70.84(11) . . . . ? _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; _audit_block_code C17H21N3S_av098_ofial _audit_creation_method 'APEX3 v2018.7-2' _shelxl_version_number ? _chemical_name_systematic ? _chemical_formula_moiety 'C17 H21 N3 S' _chemical_formula_sum 'C17 H21 N3 S' _chemical_formula_weight 299.43 #?# (Cohen, 1996) _chemical_melting_point ? #?# in K! _cell_formula_units_Z 4 #?# adjust to _chemical_formula_[] _exptl_crystal_density_diffrn 1.220 _exptl_crystal_F_000 640 #?# check! _shelx_res_file ; TITL av098_0ma_a.res in P2(1)/c av098.res created by SHELXL-2018/3 at 13:20:00 on 15-Feb-2022 REM Old TITL av098_0ma in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.112, Rweak 0.004, Alpha 0.024, Orientation as input REM Formula found by SHELXT: C17 N3 S CELL 0.71073 18.5673 5.8814 15.1443 90.000 99.720 90.000 ZERR 4.000 0.0006 0.0002 0.0006 0.000 0.001 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H N S UNIT 68 84 12 4 TEMP -100 SIZE 0.04 0.13 0.15 L.S. 10 BOND $H LIST 4 CONF ACTA SHEL 9.0 0.77 OMIT -1 0 2 ! 5.29 870.95 22.00 0.193 7.36 FMAP 2 PLAN -20 WGHT 0.034700 0.709300 FVAR 0.66234 C1 1 0.034872 0.088350 0.651767 11.00000 0.02532 0.04239 = 0.03193 -0.00058 0.00599 -0.00234 C2 1 0.059617 -0.141224 0.635561 11.00000 0.02824 0.03197 = 0.03316 0.00173 0.01203 -0.00825 AFIX 23 H2A 2 0.043277 -0.182001 0.571906 11.00000 -1.20000 H2AB 2 0.037630 -0.250829 0.672910 11.00000 -1.20000 AFIX 0 C3 1 0.180108 0.002408 0.572451 11.00000 0.02569 0.01968 = 0.02139 -0.00111 0.00859 -0.00244 C4 1 0.258491 0.077897 0.574244 11.00000 0.02150 0.02189 = 0.01880 0.00220 0.00408 -0.00153 C5 1 0.169639 0.204626 0.446172 11.00000 0.02000 0.02516 = 0.02193 0.00282 0.00309 -0.00410 C6 1 0.303981 0.306951 0.458753 11.00000 0.02042 0.02712 = 0.02113 -0.00262 0.00491 -0.00388 AFIX 43 H6 2 0.351215 0.274933 0.491386 11.00000 -1.20000 AFIX 0 C7 1 0.302148 0.458620 0.392095 11.00000 0.02207 0.02818 = 0.02242 -0.00026 0.00410 -0.00351 AFIX 43 H7 2 0.256296 0.493158 0.356432 11.00000 -1.20000 AFIX 0 C8 1 0.367416 0.573310 0.371739 11.00000 0.02664 0.02649 = 0.01689 -0.00311 0.00607 -0.00567 C9 1 0.437793 0.482361 0.392947 11.00000 0.02900 0.02936 = 0.02458 0.00194 0.00737 -0.00124 AFIX 43 H9 2 0.444450 0.337231 0.420661 11.00000 -1.20000 AFIX 0 C10 1 0.498013 0.600602 0.374176 11.00000 0.02526 0.04544 = 0.02952 0.00144 0.00540 -0.00357 AFIX 43 H10 2 0.545382 0.536108 0.389552 11.00000 -1.20000 AFIX 0 C11 1 0.489851 0.811265 0.333338 11.00000 0.03165 0.04302 = 0.02928 0.00098 0.00734 -0.01430 AFIX 43 H11 2 0.531253 0.891648 0.320523 11.00000 -1.20000 AFIX 0 C12 1 0.420624 0.903659 0.311346 11.00000 0.04057 0.03031 = 0.03021 0.00479 0.00680 -0.00930 AFIX 43 H12 2 0.414424 1.048238 0.283113 11.00000 -1.20000 AFIX 0 C13 1 0.360251 0.786545 0.330259 11.00000 0.02935 0.03045 = 0.02638 0.00298 0.00502 -0.00239 AFIX 43 H13 2 0.313087 0.852377 0.314749 11.00000 -1.20000 AFIX 0 C14 1 0.282538 0.243874 0.651515 11.00000 0.03281 0.02767 = 0.02222 -0.00220 0.00442 -0.00578 AFIX 137 H14A 2 0.329660 0.311336 0.645193 11.00000 -1.50000 H14B 2 0.287438 0.162164 0.708614 11.00000 -1.50000 H14C 2 0.245903 0.364333 0.650187 11.00000 -1.50000 AFIX 0 C15 1 0.311092 -0.123193 0.578269 11.00000 0.02786 0.02749 = 0.03430 0.00234 0.00742 0.00329 AFIX 137 H15A 2 0.359282 -0.068702 0.569575 11.00000 -1.50000 H15B 2 0.292477 -0.232294 0.530985 11.00000 -1.50000 H15C 2 0.315244 -0.197516 0.636827 11.00000 -1.50000 AFIX 0 C16 1 0.156887 0.098873 0.352645 11.00000 0.03175 0.04000 = 0.02157 -0.00145 0.00260 -0.01175 AFIX 137 H16A 2 0.174328 -0.058668 0.356377 11.00000 -1.50000 H16B 2 0.183602 0.186025 0.313456 11.00000 -1.50000 H16C 2 0.104554 0.101453 0.328131 11.00000 -1.50000 AFIX 0 C17 1 0.137495 0.443182 0.446854 11.00000 0.02871 0.02825 = 0.04613 0.00700 0.00987 0.00209 AFIX 137 H17A 2 0.150259 0.508499 0.506995 11.00000 -1.50000 H17B 2 0.084210 0.435202 0.430189 11.00000 -1.50000 H17C 2 0.157365 0.539105 0.403816 11.00000 -1.50000 AFIX 0 N1 3 0.017025 0.268602 0.666484 11.00000 0.03786 0.04882 = 0.05450 -0.00705 0.00333 0.00782 N2 3 0.133200 0.064026 0.506110 11.00000 0.02335 0.02528 = 0.02265 0.00078 0.00621 -0.00483 N3 3 0.247737 0.191671 0.486582 11.00000 0.01891 0.03110 = 0.02092 0.00622 0.00255 -0.00360 S1 4 0.158496 -0.159268 0.662175 11.00000 0.02950 0.02814 = 0.02604 0.00628 0.00992 -0.00131 HKLF 4 REM av098_0ma_a.res in P2(1)/c REM wR2 = 0.092413, GooF = S = 1.10360, Restrained GooF = 1.10360 for all data REM R1 = 0.035904 for 3312 Fo > 4sig(Fo) and 0.041877 for all 3740 data REM 194 parameters refined using 0 restraints END WGHT 0.0347 0.7093 REM Highest difference peak 0.276, deepest hole -0.217, 1-sigma level 0.041 Q1 1 0.2216 0.0396 0.5782 11.00000 0.05 0.28 Q2 1 0.1601 0.1526 0.4003 11.00000 0.05 0.25 Q3 1 0.2846 -0.0193 0.5723 11.00000 0.05 0.25 Q4 1 0.2091 0.1991 0.4680 11.00000 0.05 0.24 Q5 1 0.2662 0.1652 0.6080 11.00000 0.05 0.24 Q6 1 0.1586 0.3252 0.4443 11.00000 0.05 0.23 Q7 1 0.2556 0.1387 0.5364 11.00000 0.05 0.23 Q8 1 0.1697 -0.0642 0.6136 11.00000 0.05 0.22 Q9 1 0.1517 0.1359 0.4795 11.00000 0.05 0.22 Q10 1 0.3379 0.5198 0.3860 11.00000 0.05 0.20 Q11 1 0.3658 0.6593 0.3383 11.00000 0.05 0.20 Q12 1 0.3058 0.4434 0.4461 11.00000 0.05 0.20 Q13 1 0.3908 0.8298 0.3232 11.00000 0.05 0.16 Q14 1 0.2719 0.2633 0.4740 11.00000 0.05 0.16 Q15 1 0.1560 0.0880 0.5560 11.00000 0.05 0.16 Q16 1 0.4556 0.8754 0.3418 11.00000 0.05 0.15 Q17 1 0.3992 0.5062 0.3696 11.00000 0.05 0.15 Q18 1 0.3063 0.3251 0.4041 11.00000 0.05 0.15 Q19 1 0.3099 -0.1635 0.5173 11.00000 0.05 0.15 Q20 1 0.4036 0.5634 0.3972 11.00000 0.05 0.14 ; _shelx_res_checksum 92692 _shelx_hkl_file ; 0 0 -3 0.80 0.80 0 0 3 1.50 0.90 0 0 -3 1.30 0.90 0 0 3 0.60 0.80 0 0 3 1.10 0.80 0 0 -3 0.50 0.80 0 0 -4 9999.00 340.47 0 0 4 9621.54 339.67 0 0 -5 9.40 1.70 0 0 5 9.30 1.60 0 0 -5 8.00 1.50 0 0 -5 7.30 1.60 0 0 5 8.90 1.70 0 0 -6 4830.42 180.48 0 0 6 4755.92 179.88 0 0 7 13.00 2.40 0 0 -7 12.30 2.50 0 0 7 8.60 2.10 0 0 7 10.00 2.10 0 0 -7 9.60 2.10 0 0 -8 70.79 4.90 0 0 -8 69.59 5.10 0 0 -8 75.09 5.10 0 0 8 75.89 5.10 0 0 8 76.59 5.10 0 0 8 80.59 5.30 0 0 9 12.10 2.60 0 0 9 15.80 2.80 0 0 -9 13.90 2.70 0 0 -9 14.90 2.70 0 0 -10 821.52 31.50 0 0 -10 820.32 31.80 0 0 10 834.42 31.70 0 0 10 880.11 33.40 0 0 -10 852.21 31.80 0 0 10 773.22 31.70 0 0 -12 652.63 26.00 0 0 -12 636.04 25.40 0 0 12 598.14 25.40 0 0 12 625.14 26.20 0 0 -12 620.44 25.60 0 0 12 612.04 25.50 0 0 13 32.50 4.70 0 0 -14 86.89 7.10 0 0 -14 73.79 6.70 0 0 -14 81.99 7.00 0 0 14 105.19 7.50 0 0 -15 19.90 4.30 0 0 -15 22.80 4.20 0 0 -16 26.90 4.90 0 0 -16 23.50 5.50 0 0 16 28.20 4.90 0 0 -17 14.70 4.20 0 0 17 21.30 4.60 0 0 -17 12.80 4.00 0 0 -18 162.78 11.40 0 0 -18 153.08 11.40 0 0 18 135.19 10.70 0 0 -19 12.20 4.70 0 0 -19 17.40 5.00 0 0 19 21.70 5.20 0 1 0 0.30 0.50 0 1 0 -0.10 0.60 0 1 0 -0.60 0.50 0 -1 0 0.40 0.70 0 -1 0 -0.40 0.50 0 -1 0 0.30 0.50 0 1 -1 1222.18 42.70 0 1 1 1266.27 42.50 0 -1 1 1227.98 42.70 0 -1 -1 1268.57 42.00 0 1 2 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6.40 0 -2 -12 93.99 7.30 0 -2 12 86.19 6.30 0 2 13 5.50 2.20 0 2 13 8.20 2.60 0 2 -13 6.10 2.90 0 2 -13 4.10 2.50 0 -2 -13 10.10 2.50 0 -2 13 8.00 2.70 0 -2 -13 7.20 2.60 0 -2 13 6.60 3.10 0 -2 -13 5.00 2.90 0 2 -14 29.90 4.70 0 2 -14 24.90 5.20 0 2 14 39.60 5.10 0 2 14 29.80 4.40 0 -2 -14 25.10 4.20 0 -2 -14 25.20 5.00 0 -2 14 32.50 6.50 0 -2 -14 28.70 3.70 0 2 -15 57.89 6.10 0 2 15 52.79 6.60 0 2 15 65.79 5.70 0 2 -15 67.99 8.70 0 -2 15 60.69 7.90 0 -2 -15 64.49 5.50 0 -2 -15 49.00 7.00 0 -2 -15 68.19 6.20 0 2 -16 108.69 8.80 0 2 -16 123.19 10.10 0 2 16 131.89 8.50 0 -2 -16 120.59 9.60 0 -2 16 124.29 10.00 0 -2 -16 111.29 8.10 0 -2 -16 120.89 7.80 0 2 17 2.60 2.30 0 2 -17 -1.30 2.10 0 2 -17 -2.60 3.10 0 -2 -17 3.20 2.90 0 -2 -17 4.50 3.10 0 -2 -17 3.00 3.00 0 -2 17 5.80 3.20 0 2 -18 24.50 5.90 0 2 -18 20.70 5.70 0 2 18 23.20 4.40 0 -2 18 21.10 4.90 0 -2 -18 18.40 4.30 0 -2 -18 9.10 4.30 0 3 0 0.10 1.10 0 3 0 0.10 1.20 0 3 0 1.50 1.40 0 3 0 -1.50 1.10 0 -3 0 0.80 1.40 0 -3 0 0.90 1.20 0 3 1 1349.66 46.70 0 3 -1 1351.76 46.90 0 3 1 1330.67 46.20 0 3 -1 1255.17 46.90 0 3 1 1332.97 47.00 0 3 1 1345.57 46.40 0 3 -1 1312.97 47.10 0 3 -1 1321.67 46.60 0 3 -1 1272.57 46.60 0 -3 1 1341.77 47.40 0 -3 -1 1379.86 46.90 0 -3 -1 1331.47 46.90 0 -3 1 1320.77 46.90 0 -3 1 1304.77 46.50 0 3 2 55.79 4.20 0 3 2 58.99 3.80 0 3 2 56.19 3.50 0 3 -2 48.40 4.20 0 3 -2 52.69 4.20 0 3 -2 57.09 4.00 0 3 -2 63.59 4.70 0 3 -2 54.49 3.80 0 3 2 52.79 3.60 0 -3 -2 59.19 4.20 0 -3 2 56.39 4.20 0 -3 -2 60.19 4.00 0 3 -3 1576.14 54.59 0 3 -3 1587.24 55.79 0 3 3 1592.84 55.49 0 3 3 1563.04 53.59 0 3 -3 1590.54 55.99 0 3 -3 1575.94 54.59 0 3 3 1572.44 54.19 0 3 3 1585.34 53.89 0 3 -3 1539.95 55.89 0 -3 3 1480.95 55.39 0 -3 -3 1566.64 55.29 0 -3 -3 1551.04 54.39 0 3 4 173.58 9.20 0 3 -4 178.88 8.40 0 3 -4 183.18 8.50 0 3 4 184.58 7.50 0 3 -4 175.58 9.60 0 3 4 173.38 7.90 0 3 -4 201.08 9.80 0 -3 -4 181.08 8.20 0 -3 -4 188.18 7.60 0 -3 -4 181.78 9.10 0 3 -5 26.50 3.90 0 3 -5 36.30 4.70 0 3 5 31.00 2.20 0 3 5 31.60 3.40 0 3 -5 33.50 4.50 0 3 5 30.80 2.60 0 3 -5 26.90 3.30 0 -3 5 25.70 3.90 0 -3 -5 26.30 2.60 0 -3 -5 27.90 3.70 0 -3 -5 27.50 2.20 0 -3 5 27.80 2.80 0 3 6 51.29 3.10 0 3 6 51.89 3.60 0 3 -6 54.79 4.20 0 3 -6 54.29 4.90 0 3 -6 49.80 4.80 0 3 6 54.59 4.70 0 3 -6 56.39 5.00 0 -3 -6 55.89 4.70 0 -3 6 50.29 5.00 0 -3 -6 51.79 3.00 0 -3 -6 48.40 3.50 0 -3 6 59.99 4.10 0 3 -7 405.36 18.40 0 3 -7 405.06 18.10 0 3 7 403.66 15.00 0 3 7 394.36 17.60 0 3 -7 400.86 18.20 0 3 -7 395.46 17.70 0 3 7 399.36 16.60 0 -3 -7 393.46 17.40 0 -3 7 419.76 18.30 0 -3 7 378.26 16.10 0 -3 -7 411.56 15.70 0 -3 -7 389.56 14.80 0 3 -8 15.70 3.60 0 3 8 13.70 2.00 0 3 8 12.10 3.10 0 3 -8 20.30 3.30 0 3 -8 18.10 3.90 0 3 8 20.80 2.90 0 3 -8 23.00 4.30 0 -3 8 24.00 3.20 0 -3 -8 13.00 2.40 0 -3 -8 16.70 2.00 0 -3 -8 13.70 2.90 0 -3 8 20.70 3.90 0 3 -9 139.59 9.30 0 3 -9 130.09 8.80 0 3 9 116.59 6.80 0 3 9 117.79 8.40 0 3 9 133.49 6.40 0 3 -9 144.09 8.00 0 3 -9 112.19 8.80 0 -3 9 124.59 7.30 0 -3 -9 134.99 6.00 0 -3 -9 134.59 8.60 0 -3 -9 129.29 6.80 0 -3 9 125.09 8.80 0 3 -10 152.98 10.00 0 3 10 137.69 7.00 0 3 -10 150.98 8.70 0 3 10 142.19 7.70 0 -3 10 137.39 8.00 0 -3 -10 145.29 6.70 0 -3 10 138.19 9.60 0 -3 -10 148.09 9.40 0 -3 -10 150.58 7.60 0 3 -11 30.00 5.50 0 3 -11 26.40 4.40 0 3 11 34.70 3.80 0 3 11 27.70 3.30 0 -3 -11 28.10 4.10 0 -3 -11 30.00 4.80 0 -3 -11 32.00 4.40 0 -3 11 32.40 5.50 0 -3 11 19.80 3.60 0 3 -12 22.70 5.70 0 3 -12 24.40 4.20 0 3 12 21.10 3.00 0 3 12 21.10 3.50 0 -3 12 22.70 5.30 0 -3 -12 16.40 2.50 0 -3 -12 20.90 3.20 0 -3 12 14.20 3.00 0 3 -13 33.30 6.10 0 3 -13 41.00 5.70 0 3 13 38.90 4.90 0 3 13 41.00 3.80 0 -3 -13 41.70 4.20 0 -3 13 33.20 5.70 0 -3 -13 31.80 3.30 0 -3 -13 37.70 5.70 0 3 14 83.79 6.50 0 3 -14 86.49 8.10 0 3 -14 90.59 7.40 0 3 14 80.19 6.60 0 -3 14 81.39 7.70 0 -3 -14 88.69 7.90 0 -3 -14 91.29 5.40 0 -3 -14 91.09 6.50 0 3 -15 129.29 10.90 0 3 -15 141.49 10.10 0 3 15 146.29 8.10 0 3 15 131.19 8.90 0 -3 -15 135.59 7.50 0 -3 15 169.08 11.80 0 -3 -15 140.59 10.60 0 -3 -15 144.79 8.70 0 3 -16 60.69 8.50 0 3 -16 62.99 7.70 0 3 16 58.39 5.20 0 3 16 56.19 7.00 0 -3 -16 49.70 7.70 0 -3 16 42.90 7.10 0 -3 -16 52.39 5.20 0 -3 -16 53.79 4.90 0 3 -17 1.60 4.10 0 3 17 5.20 2.70 0 3 -17 3.90 3.00 0 -3 -17 4.00 2.60 0 -3 17 -0.80 3.60 0 -3 -17 12.50 4.10 0 4 0 62.69 4.80 0 4 0 69.79 4.80 0 4 0 72.79 4.90 0 4 0 58.99 4.80 0 -4 0 71.29 5.00 0 -4 0 61.99 5.30 0 4 -1 171.88 8.80 0 4 1 184.38 8.50 0 4 1 180.48 9.30 0 4 1 187.68 8.80 0 4 -1 187.48 9.50 0 4 -1 167.48 9.10 0 4 -1 175.18 9.00 0 4 -1 170.48 9.50 0 4 1 169.78 8.70 0 4 -1 175.18 9.10 0 -4 -1 176.28 9.20 0 -4 -1 169.38 9.00 0 -4 1 177.18 9.60 0 4 -2 108.09 6.80 0 4 -2 109.19 6.40 0 4 2 106.49 6.30 0 4 2 121.89 6.10 0 4 -2 100.09 7.00 0 4 -2 104.29 6.40 0 4 2 106.49 6.90 0 4 2 115.49 6.30 0 4 -2 104.69 6.90 0 4 -2 115.09 7.10 0 -4 -2 110.29 6.90 0 -4 -2 118.79 6.90 0 4 3 177.28 7.60 0 4 3 168.88 8.60 0 4 -3 152.78 8.20 0 4 3 169.68 8.00 0 4 3 166.08 9.00 0 4 -3 166.08 9.10 0 4 -3 153.38 9.00 0 4 -3 154.58 9.40 0 4 -3 155.68 9.10 0 4 -3 171.48 8.50 0 -4 3 159.38 9.00 0 -4 -3 149.69 8.20 0 -4 -3 146.49 8.50 0 4 4 84.09 5.10 0 4 -4 86.59 5.40 0 4 -4 78.99 5.50 0 4 4 86.99 4.90 0 4 -4 70.09 6.00 0 4 4 84.79 4.60 0 4 -4 74.49 6.00 0 4 4 89.29 7.30 0 4 -4 78.89 6.40 0 -4 4 76.19 6.10 0 -4 -4 89.49 5.50 0 -4 -4 89.59 6.20 0 4 5 6.20 1.90 0 4 -5 6.60 1.60 0 4 5 5.90 2.30 0 4 -5 2.10 1.80 0 4 5 6.30 1.60 0 4 -5 4.70 2.50 0 4 -5 4.70 2.00 0 4 5 4.00 1.30 0 -4 -5 4.00 1.80 0 -4 -5 4.70 2.30 0 -4 5 2.40 2.00 0 4 -6 100.69 6.20 0 4 -6 109.19 6.60 0 4 6 104.99 7.30 0 4 -6 99.89 7.60 0 4 -6 102.89 7.50 0 4 6 102.69 5.30 0 4 -6 94.19 7.40 0 4 6 101.89 5.10 0 4 6 101.19 5.80 0 -4 -6 99.39 6.00 0 -4 -6 94.89 6.80 0 -4 6 103.19 7.70 0 4 -7 98.49 6.40 0 4 7 94.29 4.80 0 4 7 84.79 7.80 0 4 7 91.69 5.50 0 4 -7 82.49 5.70 0 4 -7 88.09 7.10 0 4 7 100.29 4.80 0 4 -7 79.29 6.90 0 4 -7 91.09 7.40 0 -4 -7 96.69 7.10 0 -4 -7 87.69 5.50 0 -4 7 82.39 7.10 0 4 -8 1.80 2.40 0 4 -8 1.50 1.80 0 4 8 0.00 0.90 0 4 8 3.20 1.70 0 -4 -8 1.90 1.70 0 -4 -8 -1.10 1.70 0 -4 8 1.10 1.70 0 -4 8 0.20 2.20 0 -4 -8 -0.40 0.90 0 4 9 2.40 1.20 0 4 9 1.10 1.60 0 4 -9 -0.40 2.00 0 4 -9 5.00 2.10 0 -4 9 3.80 2.10 0 -4 9 3.10 2.60 0 -4 -9 -1.90 2.10 0 -4 -9 1.00 1.40 0 -4 -9 2.90 1.10 0 4 -10 33.10 4.70 0 4 10 28.20 2.50 0 4 10 23.10 3.50 0 -4 -10 32.00 3.40 0 -4 10 28.60 4.20 0 -4 -10 30.60 2.50 0 4 11 55.29 3.60 0 4 -11 51.29 7.50 0 4 11 45.70 4.40 0 4 -11 59.69 5.60 0 -4 -11 52.69 3.40 0 -4 11 57.49 7.80 0 -4 -11 49.20 6.70 0 4 -12 8.70 4.40 0 4 12 6.20 1.70 0 4 -12 6.80 3.20 0 4 12 8.80 2.60 0 -4 -12 10.10 1.70 0 -4 -12 9.00 2.90 0 -4 -12 10.60 2.60 0 -4 12 19.00 5.00 0 4 -13 34.10 6.40 0 4 -13 26.50 4.80 0 4 13 25.40 4.20 0 4 13 28.70 2.80 0 -4 -13 31.20 5.80 0 -4 13 27.60 6.00 0 -4 -13 30.50 4.10 0 -4 -13 32.50 4.30 0 4 14 25.90 4.20 0 4 14 19.00 2.60 0 4 -14 19.20 4.80 0 4 -14 18.20 5.50 0 -4 -14 19.30 3.40 0 -4 -14 28.20 5.40 0 -4 14 18.10 5.60 0 4 -15 35.00 5.80 0 4 15 25.70 3.10 0 4 15 26.20 5.00 0 4 -15 21.70 6.00 0 -4 15 33.60 6.70 0 -4 -15 35.20 6.10 0 -4 -15 32.50 4.30 0 4 -16 0.50 2.50 0 4 -16 5.60 4.20 0 4 16 0.70 1.80 0 -4 16 9.60 3.70 0 -4 -16 3.90 3.20 0 -4 -16 0.00 2.40 0 5 0 2.60 1.80 0 5 0 3.30 2.10 0 5 0 -1.20 1.40 0 5 0 0.90 1.60 0 5 0 2.20 1.60 0 5 0 1.30 1.80 0 -5 0 1.10 1.60 0 5 -1 2.70 1.90 0 5 -1 3.30 2.10 0 5 1 -0.80 1.50 0 5 -1 -0.10 1.40 0 5 1 1.10 1.90 0 5 1 -0.80 1.50 0 5 1 1.90 2.00 0 5 -1 -1.70 1.30 0 5 -1 1.80 1.90 0 5 -1 2.00 1.80 0 -5 -1 0.20 1.90 0 -5 -1 2.00 2.20 0 5 -2 440.66 18.90 0 5 2 445.46 19.70 0 5 2 452.65 18.70 0 5 -2 452.85 20.30 0 5 2 449.56 18.60 0 5 -2 430.46 19.00 0 5 -2 456.25 19.40 0 5 -2 460.05 19.90 0 -5 -2 423.56 19.00 0 -5 -2 440.56 19.20 0 5 -3 -0.90 1.30 0 5 3 -0.20 1.40 0 5 -3 -1.80 1.40 0 5 -3 -1.00 1.60 0 5 -3 0.80 1.90 0 5 -3 0.20 1.60 0 5 3 -1.30 1.40 0 5 -3 2.60 2.00 0 5 3 1.00 1.30 0 -5 -3 0.50 1.90 0 -5 -3 -1.40 1.70 0 5 4 206.28 10.00 0 5 4 213.08 9.50 0 5 -4 211.38 11.60 0 5 -4 200.88 12.10 0 5 -4 219.28 10.90 0 5 -4 211.08 10.80 0 5 -4 186.58 11.40 0 5 -4 207.28 11.80 0 5 4 198.98 9.70 0 -5 -4 212.98 10.80 0 -5 -4 204.18 11.30 0 5 -5 10.40 3.10 0 5 5 11.30 2.60 0 5 -5 3.50 2.50 0 5 5 5.20 1.90 0 5 -5 3.10 1.90 0 5 5 7.10 1.70 0 5 -5 5.90 2.20 0 -5 5 8.40 3.20 0 -5 -5 7.30 2.40 0 -5 -5 5.00 2.30 0 5 -6 25.60 3.80 0 5 -6 26.70 5.00 0 5 6 22.10 3.20 0 5 -6 20.90 3.70 0 5 6 24.00 3.40 0 5 6 22.80 2.80 0 -5 -6 21.30 3.90 0 -5 6 29.10 5.00 0 5 7 10.00 2.10 0 5 7 15.30 2.20 0 5 -7 16.80 4.20 0 5 -7 15.60 3.20 0 5 -7 22.30 3.80 0 5 7 7.70 2.40 0 -5 7 20.00 4.40 0 5 8 274.77 12.90 0 5 8 296.77 11.80 0 5 -8 282.07 14.20 0 5 -8 322.37 17.00 0 5 8 294.57 11.70 0 -5 8 292.37 16.00 0 -5 -8 302.27 15.70 0 5 -9 16.70 5.00 0 5 9 18.90 2.00 0 5 9 19.40 3.30 0 5 9 17.70 2.10 0 5 -9 22.10 4.20 0 -5 9 23.00 4.90 0 -5 -9 25.50 4.50 0 5 10 53.69 5.00 0 5 -10 82.79 6.50 0 5 -10 69.39 7.70 0 5 10 69.49 3.60 0 5 10 64.49 3.50 0 -5 -10 61.49 6.30 0 -5 -10 66.99 5.40 0 -5 10 74.49 7.70 0 5 11 4.20 1.00 0 5 -11 2.60 3.20 0 5 11 4.00 2.20 0 5 -11 1.80 2.40 0 5 11 5.10 1.00 0 -5 11 6.10 4.10 0 -5 -11 10.40 3.50 0 -5 -11 4.90 2.50 0 5 -12 40.20 5.90 0 5 -12 41.60 7.10 0 5 12 43.40 4.80 0 -5 -12 52.29 7.30 0 -5 -12 58.09 4.80 0 -5 12 55.49 7.90 0 5 13 7.00 3.00 0 5 -13 12.20 4.40 0 5 -13 21.70 4.70 0 -5 -13 15.80 4.70 0 -5 -13 12.40 3.00 0 -5 13 8.80 4.40 0 5 -14 93.39 8.80 0 5 -14 114.19 11.40 0 -5 14 120.79 10.80 0 -5 -14 115.39 7.50 0 -5 -14 134.39 10.50 0 6 0 1.40 2.10 0 6 0 3.80 2.00 0 6 0 2.50 2.50 0 6 0 1.50 2.40 0 6 0 5.50 2.60 0 6 1 112.99 7.80 0 6 1 90.19 8.20 0 6 -1 112.69 7.80 0 6 -1 100.29 8.10 0 6 1 105.69 7.40 0 6 -1 88.79 7.10 0 6 1 113.29 8.10 0 6 1 99.79 6.90 0 6 -1 100.29 7.60 0 -6 -1 103.49 7.60 0 6 2 2.90 2.00 0 6 2 1.50 2.50 0 6 2 2.30 2.20 0 6 -2 5.50 2.40 0 6 -2 2.50 2.60 0 6 2 1.60 1.50 0 6 -2 2.80 2.10 0 6 -3 74.99 7.20 0 6 3 73.09 5.70 0 6 -3 73.19 6.10 0 6 3 68.69 5.30 0 6 -3 74.99 6.50 0 6 3 72.99 5.70 0 6 3 83.39 6.70 0 -6 -3 63.39 6.20 0 -6 -3 71.39 6.40 0 6 -4 0.50 1.80 0 6 -4 -1.40 2.00 0 6 4 0.50 1.80 0 6 4 3.30 1.80 0 -6 -4 -0.70 1.80 0 -6 -4 2.60 2.50 0 6 -5 20.60 4.70 0 6 5 19.80 2.80 0 6 5 16.30 3.20 0 6 5 14.50 2.90 0 6 -5 20.40 4.20 0 6 -5 22.30 4.00 0 -6 -5 16.40 3.80 0 -6 -5 21.00 3.80 0 6 -6 3.40 2.90 0 6 6 6.80 2.50 0 6 6 7.40 2.00 0 6 6 4.30 1.80 0 6 -6 3.80 2.40 0 6 -6 8.00 3.20 0 -6 -6 7.20 2.90 0 -6 -6 8.70 3.10 0 6 7 4.00 1.50 0 6 -7 -0.70 2.10 0 6 -7 1.70 2.60 0 6 7 0.30 2.10 0 6 -7 4.00 3.50 0 6 7 1.00 1.60 0 -6 -7 0.70 2.50 0 -6 -7 2.00 2.70 0 6 -8 10.40 4.20 0 6 8 14.10 2.20 0 6 8 14.90 2.00 0 6 -8 12.10 4.00 0 6 8 10.40 3.00 0 6 -8 5.00 3.40 0 -6 -8 13.50 4.20 0 -6 -8 21.50 3.90 0 6 -9 -3.20 2.10 0 6 9 1.20 0.90 0 6 -9 -0.30 3.00 0 6 9 1.30 1.20 0 6 9 0.70 2.20 0 6 -9 5.70 3.70 0 -6 -9 0.80 2.60 0 -6 -9 0.10 2.40 0 -6 9 -0.10 2.70 0 6 -10 4.70 3.10 0 6 -10 12.80 4.80 0 6 10 3.20 2.60 0 6 -10 12.30 4.70 0 -6 -10 9.40 3.60 0 -6 -10 8.50 3.00 0 -6 10 7.50 4.00 0 6 -11 5.20 4.90 0 6 -11 2.70 3.30 0 6 -11 10.30 5.50 0 -6 -11 9.30 3.40 0 -6 11 14.40 5.90 0 6 -12 21.50 7.00 0 6 -12 16.20 4.50 0 -6 -12 15.90 4.10 0 -6 12 31.60 6.90 0 7 0 1.40 2.50 0 7 0 -0.10 2.00 0 7 -1 2.50 2.10 0 7 1 6.40 2.60 0 7 -1 -0.30 2.10 0 7 -1 1.90 3.20 0 7 1 5.10 2.80 0 7 1 2.40 2.80 0 7 2 144.79 10.20 0 7 -2 142.59 10.00 0 7 -2 151.78 10.00 0 7 2 156.18 9.00 0 7 2 163.58 10.70 0 7 2 149.19 9.60 0 7 -3 41.90 5.90 0 7 3 42.70 6.10 0 7 3 34.90 4.60 0 7 3 51.99 5.40 0 7 -3 35.10 6.30 0 7 -3 33.50 5.70 0 -7 -3 45.10 6.20 0 7 -4 4.10 3.50 0 7 4 3.40 3.00 0 7 -4 6.30 3.10 0 7 4 5.90 3.10 0 7 -4 1.40 3.10 0 7 4 -0.80 1.90 0 -7 -4 1.50 2.90 0 7 -5 13.00 3.90 0 7 5 19.50 3.60 0 7 -5 17.50 5.30 0 7 -5 17.40 3.80 0 7 5 14.50 3.80 0 7 5 11.30 2.80 0 -7 -5 18.30 4.50 0 7 6 -7.30 3.10 0 7 -6 -2.80 2.60 0 7 6 0.30 2.60 0 7 -6 -1.60 3.50 0 7 -6 0.00 3.10 0 -7 -6 2.40 3.10 0 7 -7 0.50 2.30 0 7 -7 8.60 4.20 0 7 7 3.80 1.70 0 7 7 2.80 2.70 0 7 -7 -1.40 4.10 0 -7 -7 0.70 3.70 -1 0 19 2.00 2.50 1 0 -19 -6.70 3.20 1 0 -19 1.40 3.60 1 0 -18 16.70 4.10 -1 0 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-3.60 2.50 2 -2 -16 5.00 3.00 -2 -2 16 1.10 2.50 -2 2 15 2.10 2.60 -2 2 15 3.40 2.10 2 2 -15 -0.60 2.50 2 2 -15 2.00 2.50 -2 -2 15 4.70 3.00 2 -2 -15 -3.60 2.00 2 -2 -15 -0.80 2.00 2 -2 -15 3.00 2.30 2 2 -14 63.59 6.40 -2 2 14 74.89 6.10 2 2 -14 65.69 7.10 -2 2 14 74.59 6.10 2 -2 -14 72.49 5.70 2 -2 -14 70.09 5.60 -2 -2 14 69.59 9.70 2 -2 -14 77.49 7.10 -2 2 13 160.18 9.40 -2 2 13 177.38 9.50 2 2 -13 181.08 10.70 2 2 -13 179.48 11.50 2 -2 -13 167.38 9.00 2 -2 -13 178.98 9.10 2 -2 -13 176.18 11.00 -2 -2 13 154.18 10.60 2 2 -12 4.70 2.60 2 2 -12 0.10 2.10 -2 2 12 2.00 1.80 -2 2 12 2.00 1.60 2 -2 -12 2.00 1.80 -2 -2 12 -0.30 1.50 2 -2 -12 0.20 2.10 2 -2 -12 2.60 1.60 -2 -2 12 2.60 2.70 2 2 -11 280.47 14.70 -2 2 11 275.37 14.30 2 2 -11 265.27 14.70 2 2 -11 311.87 15.40 -2 2 11 283.57 13.10 -2 2 11 289.57 12.70 2 2 -11 295.57 14.30 2 -2 -11 300.67 12.70 2 -2 -11 296.17 12.50 -2 -2 11 301.17 15.10 -2 -2 11 272.77 13.40 2 -2 -11 290.27 14.60 -2 2 10 39.90 3.50 -2 2 10 40.00 3.80 2 2 -10 42.40 4.50 2 2 -10 44.80 5.90 2 2 -10 41.10 5.00 -2 2 10 44.20 5.50 2 2 -10 39.40 5.40 -2 -2 10 44.60 5.70 2 -2 -10 44.40 3.50 -2 -2 10 45.20 4.20 2 -2 -10 36.70 3.30 2 -2 -10 35.10 4.90 2 2 -9 95.09 6.30 2 2 -9 88.29 6.70 -2 2 9 86.79 6.40 2 2 -9 91.39 6.70 -2 2 9 90.29 5.20 -2 2 9 100.29 5.70 2 2 -9 89.09 6.80 -2 -2 9 93.49 5.90 2 -2 -9 87.49 4.90 2 -2 -9 84.29 5.10 -2 -2 9 84.39 6.50 2 -2 -9 87.29 6.50 -2 2 8 37.50 3.20 2 2 -8 36.80 4.90 -2 2 8 39.50 2.90 2 2 -8 38.40 4.00 2 2 -8 32.50 4.60 2 2 -8 33.80 3.60 -2 2 8 37.70 4.70 2 -2 -8 35.10 4.50 2 -2 -8 34.00 2.70 -2 -2 8 38.50 4.80 2 -2 -8 37.00 3.00 -2 -2 8 37.50 3.40 -2 2 7 839.52 29.80 -2 2 7 806.12 31.70 2 2 -7 852.41 32.50 2 2 -7 852.01 31.40 2 2 -7 837.22 32.50 2 2 -7 864.21 32.40 -2 2 7 854.41 30.40 -2 -2 7 844.92 32.30 2 -2 -7 839.72 29.50 -2 -2 7 842.62 31.00 2 -2 -7 833.02 30.10 2 -2 -7 853.61 31.90 2 2 -6 55.89 4.80 2 2 -6 42.80 4.00 2 2 -6 47.60 3.80 -2 2 6 44.50 2.70 -2 2 6 49.10 4.20 2 2 -6 46.40 4.30 -2 2 6 49.20 3.40 2 -2 -6 44.70 3.10 2 -2 -6 43.60 2.60 2 -2 -6 46.00 4.10 -2 -2 6 43.60 3.50 -2 -2 6 46.20 4.40 -2 2 5 335.27 13.90 2 2 -5 308.87 14.20 -2 2 5 318.57 12.00 2 2 -5 321.87 14.10 2 2 -5 336.17 13.50 -2 2 5 339.77 12.80 2 2 -5 315.37 14.30 2 -2 -5 333.57 12.60 2 -2 -5 341.27 12.00 2 -2 -5 320.47 13.80 -2 -2 5 337.47 13.40 -2 -2 5 330.67 14.20 -2 2 4 714.53 24.90 -2 2 4 730.83 25.70 2 2 -4 713.83 27.40 -2 2 4 686.93 26.60 2 2 -4 692.03 27.20 2 2 -4 719.73 26.30 2 2 -4 777.02 27.20 2 -2 -4 719.63 26.60 -2 -2 4 791.62 27.40 2 -2 -4 687.13 24.90 2 -2 -4 715.83 25.60 -2 -2 4 726.23 26.30 -2 -2 4 723.63 27.40 2 2 -3 750.92 27.30 -2 2 3 767.82 27.60 -2 2 3 735.33 26.00 -2 2 3 761.32 26.70 2 2 -3 789.42 28.20 2 2 -3 746.13 27.80 -2 -2 3 776.72 27.90 2 -2 -3 790.02 27.60 -2 -2 3 735.33 28.20 2 -2 -3 743.23 26.10 2 -2 -3 734.93 26.70 2 2 -2 106.99 5.50 -2 2 2 117.09 5.30 2 2 -2 119.09 5.90 2 2 -2 123.19 6.20 -2 2 2 107.09 5.60 2 2 -2 114.49 5.60 -2 2 2 110.79 4.80 2 -2 -2 118.29 5.60 -2 -2 2 118.49 5.90 2 -2 -2 119.99 5.00 -2 -2 2 121.59 6.30 2 -2 -2 104.29 5.20 -2 2 1 1.10 0.70 2 2 -1 1.20 0.80 -2 2 1 0.50 0.80 2 2 -1 0.30 1.00 -2 2 1 0.70 0.80 2 2 -1 -0.40 0.80 2 2 -1 0.60 0.90 -2 2 1 -0.10 0.70 -2 -2 1 -0.10 0.80 -2 -2 1 -0.20 1.10 2 -2 -1 1.30 1.00 2 -2 -1 -0.10 0.70 2 2 0 85.09 4.60 2 2 0 87.39 4.60 -2 2 0 86.19 4.50 -2 2 0 92.09 4.50 -2 2 0 91.49 4.70 -2 2 0 85.49 4.20 2 2 0 85.69 4.20 -2 2 0 92.39 4.50 -2 -2 0 82.09 4.20 -2 -2 0 87.69 4.80 -2 -2 0 78.59 4.50 2 -2 0 75.69 4.50 2 -2 0 82.69 4.10 -2 2 -1 642.04 23.60 -2 2 -1 653.53 23.60 -2 2 -1 637.14 22.80 2 2 1 628.44 23.60 -2 2 -1 692.33 23.90 2 2 1 650.83 22.50 -2 2 -1 660.23 23.70 2 2 1 657.63 23.40 -2 -2 -1 606.74 22.40 2 -2 1 628.24 22.70 -2 -2 -1 620.54 23.50 -2 -2 -1 655.73 23.60 -2 2 -2 45.90 3.40 2 2 2 44.80 3.10 2 2 2 43.60 2.20 -2 2 -2 42.70 2.60 -2 2 -2 47.30 3.50 2 2 2 44.70 2.10 2 2 2 43.60 3.20 -2 2 -2 47.90 2.70 -2 -2 -2 44.90 3.10 2 -2 2 45.10 3.50 2 -2 2 44.30 3.50 -2 -2 -2 39.00 3.10 -2 2 -3 146.89 7.40 -2 2 -3 152.68 7.60 2 2 3 143.29 6.70 -2 2 -3 147.09 6.20 2 2 3 144.89 7.20 2 2 3 142.79 5.30 2 2 3 146.59 5.20 2 -2 3 141.19 7.30 2 -2 3 145.49 6.20 -2 -2 -3 146.49 6.80 2 -2 3 143.39 7.40 -2 -2 -3 138.19 7.00 2 2 4 39.50 1.60 -2 2 -4 44.00 3.90 2 2 4 39.10 3.60 2 2 4 40.00 3.10 -2 2 -4 36.50 2.70 -2 2 -4 42.90 3.60 2 -2 4 42.00 3.60 2 -2 4 37.20 3.70 -2 -2 -4 40.20 3.20 -2 -2 -4 36.50 3.50 2 -2 4 38.40 2.60 2 2 5 32.50 3.40 -2 2 -5 33.20 4.00 -2 2 -5 41.10 4.00 2 2 5 33.40 3.90 -2 2 -5 33.10 2.60 2 2 5 32.80 1.80 -2 -2 -5 37.50 3.40 -2 -2 -5 34.40 1.60 2 -2 5 29.20 3.80 -2 -2 -5 30.80 2.80 2 -2 5 34.40 2.60 2 -2 5 30.50 3.80 2 2 6 355.66 12.60 2 2 6 331.77 15.00 -2 2 -6 352.76 14.00 -2 2 -6 367.06 15.70 2 2 6 356.86 14.30 2 -2 6 337.07 15.50 -2 -2 -6 350.56 14.20 2 -2 6 371.76 17.00 -2 -2 -6 347.77 12.40 2 -2 6 339.37 14.40 -2 2 -7 68.29 4.70 -2 2 -7 72.99 5.80 -2 2 -7 76.39 5.60 2 2 7 73.19 4.90 2 2 7 68.19 3.60 2 2 7 72.59 5.40 -2 -2 -7 77.79 3.50 2 -2 7 78.19 5.70 2 -2 7 83.09 6.00 -2 -2 -7 73.09 4.90 2 -2 7 78.49 4.50 -2 -2 -7 74.69 5.30 -2 2 -8 678.13 27.00 2 2 8 615.84 25.20 2 2 8 678.73 23.80 -2 2 -8 667.13 25.20 -2 2 -8 705.83 27.10 2 2 8 636.04 26.20 -2 -2 -8 655.43 25.10 2 -2 8 662.73 24.80 2 -2 8 676.13 26.80 -2 -2 -8 636.54 26.00 -2 -2 -8 671.13 23.50 2 -2 8 681.63 27.20 2 2 9 81.89 4.40 -2 2 -9 70.49 5.30 2 2 9 77.29 5.50 -2 2 -9 81.59 6.60 2 2 9 80.49 7.00 -2 2 -9 90.79 7.70 2 -2 9 74.29 5.00 -2 -2 -9 66.29 5.80 2 -2 9 80.29 6.40 2 -2 9 78.09 7.50 -2 -2 -9 76.99 4.10 -2 -2 -9 86.39 5.70 2 2 10 159.78 7.50 2 2 10 140.09 9.20 -2 2 -10 159.78 8.70 -2 2 -10 159.58 9.80 -2 2 -10 149.39 9.80 2 2 10 138.39 8.30 -2 -2 -10 159.88 8.50 -2 -2 -10 153.48 7.20 2 -2 10 170.38 8.40 2 -2 10 168.58 10.00 -2 -2 -10 154.08 9.40 2 -2 10 169.48 10.20 2 2 11 7.70 2.20 -2 2 -11 3.60 2.00 2 2 11 5.20 1.80 -2 2 -11 4.80 2.90 2 2 11 3.70 2.50 -2 2 -11 6.20 2.90 -2 -2 -11 8.70 2.50 2 -2 11 7.10 2.30 -2 -2 -11 3.80 2.10 2 -2 11 5.10 2.80 -2 -2 -11 6.50 1.70 -2 2 -12 94.59 6.70 -2 2 -12 86.79 7.60 2 2 12 96.99 7.10 2 2 12 80.39 5.50 2 -2 12 82.99 7.10 -2 -2 -12 83.39 6.30 2 -2 12 83.39 7.10 -2 -2 -12 105.49 7.70 -2 -2 -12 92.69 5.40 2 2 13 39.10 5.40 -2 2 -13 29.00 4.60 2 2 13 32.20 4.00 -2 2 -13 31.40 5.80 -2 -2 -13 29.40 4.50 2 -2 13 30.60 4.50 2 -2 13 27.20 5.20 -2 -2 -13 30.40 5.00 -2 -2 -13 32.50 3.40 2 2 14 34.00 5.40 2 2 14 22.10 3.50 -2 2 -14 28.30 4.40 -2 2 -14 28.60 5.30 -2 -2 -14 37.80 5.30 -2 -2 -14 36.30 5.80 -2 -2 -14 26.40 3.60 2 -2 14 25.50 5.20 2 2 15 109.69 7.30 -2 2 -15 117.89 9.80 -2 2 -15 126.69 9.10 -2 -2 -15 113.69 7.10 -2 -2 -15 119.49 8.30 2 -2 15 117.69 9.60 -2 -2 -15 128.89 9.40 2 2 16 47.40 4.80 -2 2 -16 52.99 6.60 -2 2 -16 59.29 8.10 2 -2 16 57.19 7.90 -2 -2 -16 48.10 4.90 -2 -2 -16 58.09 6.40 -2 -2 -16 56.99 7.70 2 2 17 22.60 4.00 -2 2 -17 24.60 5.60 -2 2 -17 24.30 5.30 2 -2 17 18.40 5.40 -2 -2 -17 20.60 4.70 -2 -2 -17 18.60 4.00 -2 -2 -17 16.10 4.40 2 2 18 6.60 2.80 -2 2 -18 15.90 4.30 2 -2 18 13.20 5.50 -2 -2 -18 15.10 4.80 -2 -2 -18 1.50 3.50 2 3 -18 2.50 3.80 2 3 -18 6.90 4.90 -2 3 18 -1.40 2.40 2 -3 -18 0.60 4.00 -2 -3 18 4.10 4.00 2 -3 -18 10.30 3.30 -2 3 17 92.79 7.60 2 3 -17 111.19 10.40 -2 3 17 94.59 7.20 2 3 -17 92.19 9.50 2 -3 -17 92.69 8.90 2 -3 -17 101.19 7.00 2 -3 -17 100.19 7.70 -2 -3 17 95.09 10.00 2 3 -16 5.50 3.10 2 3 -16 8.60 4.50 -2 3 16 7.30 3.30 -2 3 16 11.60 3.00 -2 -3 16 6.80 4.10 2 -3 -16 11.00 3.90 2 -3 -16 10.80 3.20 2 -3 -16 9.50 2.50 -2 3 15 27.70 4.40 2 3 -15 18.50 4.60 -2 3 15 22.60 4.00 2 3 -15 24.20 5.80 -2 -3 15 21.50 4.80 2 -3 -15 26.10 3.80 2 -3 -15 24.60 3.60 2 -3 -15 29.10 5.50 -2 3 14 88.19 6.60 2 3 -14 75.19 8.20 -2 3 14 86.29 6.40 2 -3 -14 91.19 6.00 2 -3 -14 96.49 8.50 2 -3 -14 89.29 5.90 -2 -3 14 110.79 9.00 2 3 -13 47.50 6.40 -2 3 13 43.20 4.30 -2 3 13 50.19 4.40 2 3 -13 52.39 7.40 2 -3 -13 44.50 6.40 2 -3 -13 40.90 4.00 -2 -3 13 48.50 7.00 2 -3 -13 46.00 4.10 -2 3 12 -2.60 1.50 -2 3 12 -1.50 1.90 2 3 -12 0.50 2.20 2 3 -12 -0.50 1.80 2 -3 -12 -0.10 1.30 -2 -3 12 -2.10 2.00 2 -3 -12 0.80 1.90 2 -3 -12 0.70 1.40 -2 3 11 67.09 4.70 -2 3 11 74.09 5.20 2 3 -11 63.79 6.90 2 3 -11 72.89 6.20 2 -3 -11 72.79 4.60 -2 -3 11 83.99 7.40 -2 -3 11 68.09 5.50 2 -3 -11 64.79 6.30 2 -3 -11 75.19 4.80 2 3 -10 18.30 3.70 -2 3 10 17.80 2.90 2 3 -10 12.90 3.90 2 -3 -10 14.90 2.40 -2 -3 10 10.40 3.00 -2 -3 10 13.40 3.10 2 -3 -10 11.80 3.10 2 -3 -10 16.60 2.30 -2 3 9 25.50 4.30 2 3 -9 33.90 5.30 -2 3 9 29.30 3.00 2 3 -9 34.80 5.20 2 3 -9 21.60 4.10 2 3 -9 33.60 4.60 -2 3 9 26.50 3.00 -2 -3 9 30.10 4.80 2 -3 -9 28.70 2.70 2 -3 -9 25.40 2.40 2 -3 -9 30.30 4.40 -2 -3 9 27.10 3.70 -2 3 8 31.20 4.30 2 3 -8 39.10 5.10 2 3 -8 34.70 4.40 -2 3 8 31.60 2.90 -2 3 8 28.70 2.60 2 3 -8 31.40 4.90 2 3 -8 37.90 5.30 -2 -3 8 30.90 4.90 2 -3 -8 30.30 4.50 -2 -3 8 28.40 3.70 2 -3 -8 29.70 2.70 2 -3 -8 27.60 2.40 -2 3 7 24.30 2.90 -2 3 7 20.70 2.00 2 3 -7 23.80 3.60 2 3 -7 27.70 4.20 2 3 -7 22.90 4.00 -2 3 7 21.70 3.60 2 3 -7 22.70 4.00 2 -3 -7 23.10 2.10 -2 -3 7 20.50 3.90 -2 -3 7 23.30 3.30 2 -3 -7 28.00 4.00 -2 3 6 409.26 16.10 2 3 -6 428.36 18.70 -2 3 6 397.66 17.80 2 3 -6 418.86 18.70 -2 3 6 416.86 15.50 2 3 -6 436.06 18.40 2 3 -6 409.76 17.20 -2 -3 6 435.96 18.40 -2 -3 6 401.66 16.90 2 -3 -6 424.26 16.10 2 -3 -6 420.06 15.60 2 -3 -6 430.36 17.80 2 3 -5 1922.71 72.09 -2 3 5 2096.49 69.89 -2 3 5 2084.69 71.69 2 3 -5 2049.70 71.99 2 3 -5 2004.90 72.39 -2 3 5 2014.60 69.09 2 -3 -5 1990.70 69.19 2 -3 -5 2047.50 71.49 2 -3 -5 2035.10 69.79 -2 -3 5 2084.79 72.09 -2 -3 5 2057.49 70.79 2 3 -4 211.18 10.30 2 3 -4 194.48 9.50 -2 3 4 206.98 8.30 2 3 -4 202.88 9.40 -2 3 4 206.68 10.00 2 3 -4 194.78 10.50 2 3 -4 213.58 10.60 -2 3 4 204.78 8.80 -2 -3 4 203.78 10.70 2 -3 -4 197.18 9.70 2 -3 -4 197.58 8.40 2 -3 -4 212.08 8.90 -2 -3 4 208.48 10.20 -2 3 3 41.50 2.80 2 3 -3 42.50 3.50 -2 3 3 42.50 3.20 -2 3 3 39.90 3.60 2 3 -3 49.50 3.80 2 3 -3 50.19 4.30 2 3 -3 42.20 3.90 -2 -3 3 44.40 4.30 2 -3 -3 54.29 4.00 2 -3 -3 50.49 3.40 -2 -3 3 44.40 4.00 2 -3 -3 44.30 3.10 2 3 -2 15.90 2.80 -2 3 2 13.00 2.40 2 3 -2 15.00 2.40 2 3 -2 13.10 2.30 2 3 -2 11.80 2.40 -2 3 2 11.40 1.90 -2 3 2 14.90 2.10 2 -3 -2 12.60 2.30 -2 -3 2 18.70 3.20 2 -3 -2 11.90 2.00 -2 -3 2 14.10 2.50 2 3 -1 185.38 9.20 -2 3 1 188.08 8.80 -2 3 1 202.98 8.80 -2 3 1 182.88 8.30 -2 3 1 187.18 8.50 2 3 -1 185.58 8.80 2 3 -1 173.68 8.60 -2 3 1 189.58 8.60 2 -3 -1 195.98 8.60 -2 -3 1 175.68 9.20 -2 -3 1 187.58 8.60 2 3 0 488.05 19.40 2 3 0 531.05 19.70 -2 3 0 506.95 19.50 -2 3 0 490.65 19.00 -2 3 0 493.35 19.20 2 3 0 463.05 18.60 -2 3 0 511.95 19.20 -2 3 0 418.26 18.50 -2 -3 0 502.05 19.30 2 -3 0 518.45 18.80 -2 -3 0 511.45 18.70 -2 -3 0 520.15 19.80 -2 3 -1 624.94 24.60 -2 3 -1 709.43 25.90 -2 3 -1 717.53 25.80 -2 3 -1 669.43 25.50 2 3 1 671.73 25.30 2 3 1 672.43 25.60 2 3 1 669.13 24.30 2 3 1 711.93 24.60 -2 3 -1 678.63 25.60 -2 3 -1 698.03 24.70 2 -3 1 654.93 24.60 -2 -3 -1 650.13 25.40 -2 -3 -1 668.73 25.50 -2 3 -2 352.46 14.80 2 3 2 351.66 14.20 -2 3 -2 344.57 13.70 -2 3 -2 359.86 15.00 -2 3 -2 345.77 14.90 -2 3 -2 360.66 15.10 -2 3 -2 376.66 14.70 2 3 2 351.36 13.00 2 3 2 330.37 13.10 2 3 2 344.57 14.80 -2 -3 -2 349.77 14.50 -2 -3 -2 333.77 14.70 -2 3 -3 50.59 3.40 -2 3 -3 43.50 4.00 2 3 3 52.09 3.80 2 3 3 48.30 2.70 2 3 3 49.60 4.00 -2 3 -3 42.80 4.10 -2 3 -3 44.50 4.20 -2 3 -3 53.79 5.00 -2 3 -3 49.90 3.30 2 3 3 49.70 2.60 2 -3 3 49.00 4.90 -2 -3 -3 45.30 3.80 -2 -3 -3 49.20 4.10 -2 3 -4 73.79 5.70 2 3 4 80.89 5.70 2 3 4 77.89 3.50 -2 3 -4 79.29 4.50 -2 3 -4 80.09 4.50 2 3 4 83.59 3.40 2 3 4 77.59 4.90 -2 3 -4 76.19 5.60 -2 -3 -4 85.99 5.20 2 -3 4 80.29 5.80 -2 -3 -4 74.79 5.40 2 3 5 789.22 28.90 2 3 5 790.02 30.30 -2 3 -5 797.22 28.70 -2 3 -5 753.12 30.50 2 3 5 816.42 26.80 -2 3 -5 803.02 28.50 -2 3 -5 763.82 30.50 -2 3 -5 748.33 30.60 2 3 5 769.82 26.80 2 -3 5 800.52 30.60 2 -3 5 784.32 28.50 -2 -3 -5 811.82 29.20 -2 -3 -5 781.82 30.00 2 3 6 29.40 1.50 -2 3 -6 30.50 2.90 2 3 6 25.60 3.80 -2 3 -6 36.60 4.80 -2 3 -6 28.10 4.40 2 3 6 27.70 3.00 -2 3 -6 38.80 5.10 2 -3 6 36.90 4.90 2 -3 6 34.80 4.70 -2 -3 -6 28.80 4.20 -2 -3 -6 30.50 3.00 2 -3 6 30.70 2.80 2 3 7 97.99 5.90 2 3 7 90.39 7.60 -2 3 -7 103.49 6.00 -2 3 -7 106.89 8.50 -2 3 -7 93.79 7.10 2 3 7 94.99 4.10 2 -3 7 104.59 5.70 -2 -3 -7 103.09 6.80 -2 -3 -7 99.49 3.80 -2 -3 -7 91.79 5.80 2 -3 7 106.39 7.50 2 3 8 38.30 2.10 -2 3 -8 38.20 4.10 2 3 8 39.20 5.20 -2 3 -8 40.70 5.30 -2 3 -8 39.30 5.30 -2 3 -8 40.40 5.70 2 3 8 30.90 3.50 -2 -3 -8 40.80 5.10 -2 -3 -8 32.80 3.50 2 -3 8 31.20 4.80 2 -3 8 43.60 5.80 -2 -3 -8 37.40 1.90 2 -3 8 33.50 3.20 -2 3 -9 23.70 4.30 2 3 9 29.60 1.90 2 3 9 23.40 4.40 -2 3 -9 27.10 4.90 2 3 9 21.90 3.50 -2 3 -9 33.60 5.40 -2 3 -9 26.10 3.70 2 -3 9 23.20 3.20 -2 -3 -9 27.00 3.60 -2 -3 -9 21.30 3.80 -2 -3 -9 23.80 1.70 2 -3 9 22.40 4.40 2 -3 9 24.40 4.40 -2 3 -10 1.20 2.40 2 3 10 -0.80 1.30 2 3 10 0.00 0.70 -2 3 -10 -2.30 1.40 -2 -3 -10 0.80 1.60 -2 -3 -10 -0.60 1.50 2 -3 10 0.40 2.30 2 -3 10 1.20 1.50 -2 -3 -10 0.40 0.80 2 3 11 2.30 1.10 -2 3 -11 3.50 2.30 -2 3 -11 0.40 2.10 2 3 11 -1.20 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5.30 2.50 2 -4 -16 0.60 2.30 -2 -4 16 3.50 4.10 2 -4 -16 5.20 3.70 -2 4 15 0.60 2.10 2 4 -15 0.80 3.00 -2 4 15 0.10 2.40 2 -4 -15 9.80 3.20 2 -4 -15 0.30 2.40 -2 -4 15 -0.50 3.50 -2 4 14 11.90 2.70 -2 4 14 12.20 3.10 2 4 -14 17.00 5.00 2 4 -14 15.60 4.80 -2 -4 14 13.90 4.20 2 -4 -14 22.90 3.10 2 -4 -14 22.40 3.30 2 -4 -14 14.80 3.90 2 4 -13 214.38 14.00 -2 4 13 185.18 9.50 2 4 -13 193.48 12.40 -2 -4 13 215.18 14.00 2 -4 -13 217.88 13.20 2 -4 -13 195.08 9.50 2 -4 -13 216.98 9.70 -2 4 12 81.39 5.30 2 4 -12 94.79 8.90 2 4 -12 83.69 7.40 -2 4 12 69.09 5.20 2 -4 -12 82.19 5.00 -2 -4 12 86.99 8.00 2 -4 -12 75.99 7.50 2 -4 -12 74.79 5.10 2 4 -11 59.89 5.70 -2 4 11 57.79 4.20 2 4 -11 64.69 7.10 -2 4 11 65.59 4.80 2 -4 -11 60.69 6.20 2 -4 -11 61.09 4.30 -2 -4 11 72.19 7.30 2 -4 -11 60.59 4.30 -2 4 10 10.80 2.10 2 4 -10 7.70 2.60 2 4 -10 9.30 4.20 2 -4 -10 9.70 2.00 2 -4 -10 6.20 1.80 -2 -4 10 5.70 2.50 2 -4 -10 7.50 2.70 -2 4 9 2.30 1.30 -2 4 9 1.60 1.50 2 4 -9 1.10 1.90 2 4 -9 1.60 2.20 2 -4 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10.90 2 4 -4 230.98 12.30 2 4 -4 268.37 12.00 2 4 -4 233.78 12.70 -2 4 4 238.88 12.20 -2 4 4 249.48 11.30 -2 4 4 266.47 10.70 2 -4 -4 253.47 12.20 -2 -4 4 249.78 12.50 2 -4 -4 265.57 11.10 -2 4 3 26.10 2.70 -2 4 3 29.40 3.60 2 4 -3 23.70 3.50 2 4 -3 31.30 4.60 2 4 -3 30.00 4.40 2 4 -3 30.50 3.90 -2 4 3 27.70 2.70 2 4 -3 32.20 4.40 -2 4 3 28.60 4.00 2 -4 -3 23.70 3.20 -2 -4 3 29.90 4.20 2 -4 -3 22.80 3.50 -2 -4 3 28.50 4.60 2 4 -2 31.10 3.80 2 4 -2 34.20 3.80 -2 4 2 29.50 3.70 2 4 -2 33.60 4.10 2 4 -2 31.50 3.90 -2 4 2 28.80 3.10 -2 4 2 29.00 3.00 -2 4 2 27.60 2.90 -2 4 2 33.70 3.50 -2 -4 2 29.50 4.30 -2 -4 2 30.80 4.50 2 -4 -2 26.40 3.50 2 4 -1 68.79 5.20 2 4 -1 68.89 5.10 -2 4 1 74.39 4.90 2 4 -1 76.59 5.10 -2 4 1 67.69 5.00 -2 4 1 64.39 4.90 -2 4 1 75.19 5.00 2 4 -1 73.39 5.20 -2 4 1 83.99 5.50 2 4 -1 64.59 5.20 -2 -4 1 89.69 5.40 -2 -4 1 64.89 5.60 2 -4 -1 71.49 5.00 -2 4 0 25.10 3.60 -2 4 0 18.70 2.80 -2 4 0 19.10 3.00 2 4 0 17.00 2.90 2 4 0 19.00 2.80 -2 4 0 19.90 3.00 2 4 0 16.10 2.90 -2 4 0 18.80 3.10 2 4 0 19.70 2.80 2 -4 0 17.40 2.80 -2 -4 0 15.50 2.90 -2 -4 0 20.00 3.50 -2 4 -1 3.70 1.80 -2 4 -1 3.10 1.30 -2 4 -1 3.80 1.60 2 4 1 4.60 1.50 2 4 1 2.60 1.70 2 4 1 5.00 1.60 -2 4 -1 3.90 2.00 2 4 1 3.90 1.70 -2 4 -1 3.10 1.60 -2 4 -1 1.50 1.60 -2 -4 -1 4.40 2.00 -2 -4 -1 3.30 1.80 -2 4 -2 3.50 1.40 2 4 2 -0.30 1.30 2 4 2 0.90 1.20 -2 4 -2 -0.50 1.20 -2 4 -2 1.50 1.30 -2 4 -2 0.40 1.30 2 4 2 0.80 0.90 -2 4 -2 1.80 1.50 2 4 2 1.40 1.50 -2 4 -2 0.10 1.30 -2 -4 -2 3.00 1.80 -2 4 -3 398.16 17.30 -2 4 -3 380.46 17.50 -2 4 -3 370.46 17.40 -2 4 -3 390.26 16.10 2 4 3 403.86 14.80 2 4 3 420.66 15.30 -2 4 -3 388.16 16.00 2 4 3 381.56 16.20 -2 4 -3 385.06 17.40 -2 -4 -3 392.96 17.10 -2 -4 -3 396.56 16.90 2 4 4 148.49 7.00 -2 4 -4 173.18 10.00 -2 4 -4 168.78 8.30 -2 4 -4 169.78 9.20 2 4 4 164.08 9.40 2 4 4 164.58 8.40 -2 4 -4 157.38 9.60 -2 4 -4 173.78 9.70 2 4 4 168.78 6.80 -2 -4 -4 175.68 9.00 -2 -4 -4 151.68 9.00 -2 4 -5 20.60 4.20 2 4 5 21.00 1.60 -2 4 -5 23.60 4.20 -2 4 -5 16.90 2.80 -2 4 -5 19.60 3.00 2 4 5 26.50 3.60 -2 4 -5 15.90 3.60 2 4 5 16.20 1.70 -2 4 -5 26.20 4.20 2 4 5 22.20 3.70 2 -4 5 18.00 3.50 -2 -4 -5 15.10 3.20 -2 -4 -5 24.20 3.50 -2 4 -6 4.40 1.80 2 4 6 5.30 1.90 2 4 6 3.10 0.70 -2 4 -6 -3.10 1.80 -2 4 -6 0.60 1.60 -2 4 -6 3.90 1.60 -2 4 -6 4.40 2.30 2 4 6 3.60 0.70 2 4 6 1.70 1.60 -2 4 -6 0.60 1.50 2 -4 6 1.30 2.30 -2 -4 -6 5.50 2.30 2 4 7 177.08 9.10 -2 4 -7 178.48 8.90 -2 4 -7 195.68 9.40 -2 4 -7 175.98 11.10 -2 4 -7 162.28 12.10 -2 -4 -7 173.68 10.30 2 -4 7 170.28 10.70 -2 -4 -7 168.58 9.10 -2 4 -8 46.70 4.10 -2 4 -8 50.39 4.60 -2 4 -8 48.40 6.70 2 4 8 54.59 4.50 2 -4 8 36.60 3.90 -2 -4 -8 51.99 5.20 2 -4 8 42.90 6.40 -2 -4 -8 46.90 4.20 -2 4 -9 12.40 2.90 2 4 9 13.10 2.70 -2 4 -9 15.60 4.00 -2 -4 -9 15.80 3.70 2 -4 9 14.40 2.70 2 -4 9 13.00 3.80 -2 -4 -9 14.00 3.10 2 4 10 0.30 2.00 -2 4 -10 7.40 3.00 -2 4 -10 4.30 2.30 2 -4 10 5.30 2.50 2 -4 10 4.40 2.20 -2 -4 -10 7.00 3.00 -2 -4 -10 5.00 2.20 -2 4 -11 132.29 10.40 -2 4 -11 149.88 9.10 2 4 11 148.59 8.60 2 -4 11 147.49 10.80 2 -4 11 135.49 8.10 -2 -4 -11 139.99 10.00 -2 -4 -11 134.49 8.30 -2 4 -12 20.00 4.00 -2 4 -12 16.40 4.70 2 4 12 10.10 3.40 2 -4 12 17.50 4.40 -2 -4 -12 18.70 3.60 -2 -4 -12 17.50 4.70 2 -4 12 18.40 3.70 2 4 13 33.90 5.10 -2 4 -13 28.00 5.90 -2 4 -13 47.60 6.00 -2 -4 -13 43.30 6.50 2 -4 13 40.10 6.40 -2 -4 -13 37.20 4.90 -2 4 -14 11.10 3.10 2 4 14 6.10 3.40 -2 4 -14 5.90 3.70 -2 -4 -14 12.00 3.00 2 -4 14 10.80 3.40 -2 -4 -14 14.00 4.20 -2 4 -15 31.30 6.80 -2 4 -15 39.20 5.90 2 -4 15 28.90 6.50 -2 -4 -15 33.60 6.40 -2 -4 -15 44.60 5.50 -2 4 -16 21.80 6.40 -2 4 -16 32.70 5.40 2 -4 16 36.50 6.90 -2 -4 -16 29.40 6.40 -2 -4 -16 25.40 4.50 2 5 -14 41.40 6.40 -2 5 14 33.80 3.70 2 5 -14 32.40 8.90 2 -5 -14 56.09 4.50 -2 -5 14 41.70 9.50 -2 5 13 5.10 3.10 2 5 -13 2.20 3.90 2 5 -13 9.60 3.60 -2 5 13 2.90 1.90 2 -5 -13 6.00 3.50 -2 -5 13 3.70 3.70 2 -5 -13 6.60 2.00 2 -5 -13 9.00 2.70 2 5 -12 8.60 3.30 2 5 -12 10.50 4.30 -2 5 12 10.60 2.50 2 -5 -12 12.60 2.30 2 -5 -12 8.70 2.40 2 -5 -12 12.90 3.70 -2 -5 12 12.00 3.80 2 5 -11 104.89 8.10 2 5 -11 109.79 9.60 -2 5 11 100.49 6.00 2 -5 -11 102.89 6.00 2 -5 -11 100.79 8.30 -2 -5 11 90.09 8.60 2 -5 -11 106.09 5.80 -2 5 10 235.28 10.50 -2 5 10 228.08 12.00 2 5 -10 223.38 14.50 2 5 -10 221.98 12.90 2 -5 -10 223.18 13.30 2 -5 -10 232.78 10.20 -2 -5 10 222.28 14.10 2 -5 -10 212.18 10.00 -2 5 9 0.10 1.40 2 5 -9 -1.00 2.30 -2 5 9 4.80 1.70 -2 5 9 0.80 1.50 2 5 -9 1.70 2.20 2 -5 -9 -1.50 1.70 2 -5 -9 3.70 1.80 -2 -5 9 1.60 2.30 -2 5 8 7.00 1.90 -2 5 8 7.10 2.10 -2 5 8 6.20 2.00 2 5 -8 7.10 2.80 2 5 -8 3.50 2.90 2 -5 -8 11.30 3.40 2 -5 -8 3.60 1.90 -2 5 7 43.90 3.90 -2 5 7 40.60 3.60 2 5 -7 47.80 7.10 -2 5 7 35.60 3.40 2 5 -7 44.90 5.50 2 -5 -7 37.80 3.70 2 -5 -7 38.10 5.40 -2 -5 7 33.10 5.50 -2 5 6 370.56 15.60 -2 5 6 359.46 15.10 -2 5 6 347.67 14.70 2 5 -6 362.46 18.60 2 5 -6 364.66 16.70 2 -5 -6 362.36 15.20 2 -5 -6 370.56 17.40 -2 -5 6 388.86 18.20 -2 5 5 185.98 9.80 2 5 -5 196.98 10.80 2 5 -5 179.78 11.20 -2 5 5 202.08 9.30 2 5 -5 208.98 12.50 2 5 -5 210.38 11.00 -2 -5 5 209.78 11.70 2 -5 -5 207.68 11.20 2 -5 -5 195.28 9.70 2 5 -4 14.30 3.20 -2 5 4 15.70 2.80 -2 5 4 12.70 2.90 -2 5 4 11.70 2.20 -2 5 4 14.00 2.80 -2 5 4 23.00 3.90 2 5 -4 12.70 2.90 2 5 -4 13.00 3.10 2 5 -4 21.10 4.40 -2 -5 4 14.80 3.60 2 -5 -4 15.00 2.90 2 -5 -4 15.70 3.50 2 5 -3 7.50 3.00 -2 5 3 10.30 3.10 2 5 -3 12.20 2.90 2 5 -3 6.10 2.00 -2 5 3 8.70 2.40 -2 5 3 7.70 2.00 2 5 -3 8.70 3.30 -2 5 3 9.70 2.60 2 5 -3 7.70 2.40 2 5 -3 11.10 3.00 -2 5 3 12.30 2.70 2 -5 -3 8.90 2.70 -2 -5 3 10.20 3.10 -2 5 2 24.40 3.70 -2 5 2 23.10 4.20 2 5 -2 19.50 3.70 2 5 -2 27.60 4.80 -2 5 2 26.30 4.10 2 5 -2 24.00 3.70 2 5 -2 23.60 4.00 2 5 -2 23.00 3.70 -2 5 2 18.60 3.20 -2 5 2 23.40 3.60 2 5 -2 16.40 3.60 2 -5 -2 14.40 3.20 -2 -5 2 27.10 4.70 2 5 -1 3.90 2.30 -2 5 1 0.40 1.30 2 5 -1 -0.60 1.40 -2 5 1 1.20 1.90 2 5 -1 0.60 1.70 -2 5 1 0.40 1.60 2 5 -1 2.90 2.00 2 5 -1 3.70 2.00 -2 5 1 1.60 1.90 -2 5 1 3.30 1.90 2 -5 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4 1 6.50 1.70 -4 4 -1 7.10 2.50 4 4 1 7.00 1.70 -4 4 -1 12.90 2.70 4 4 1 7.80 2.20 4 4 1 10.20 2.40 -4 4 -1 8.30 1.90 -4 4 -1 6.10 1.60 -4 -4 -1 8.50 2.40 -4 -4 -1 6.80 2.40 -4 4 -2 21.50 3.00 -4 4 -2 22.10 2.80 -4 4 -2 17.70 3.40 4 4 2 23.20 2.20 4 4 2 20.70 3.20 4 4 2 29.60 4.20 -4 4 -2 27.80 4.20 4 4 2 17.10 2.10 -4 4 -2 24.30 3.80 -4 4 -2 21.50 3.40 -4 -4 -2 25.70 3.70 -4 -4 -2 25.50 3.90 -4 4 -3 108.19 5.90 -4 4 -3 108.59 6.00 -4 4 -3 102.99 7.40 -4 4 -3 120.49 7.70 4 4 3 116.89 7.50 4 4 3 117.49 5.00 -4 4 -3 110.39 7.40 4 4 3 110.39 6.80 4 4 3 103.49 4.70 -4 4 -3 110.59 7.40 -4 -4 -3 104.19 7.00 -4 -4 -3 95.69 6.90 -4 4 -4 18.30 3.80 4 4 4 25.30 3.50 4 4 4 20.40 1.20 -4 4 -4 23.50 4.00 -4 4 -4 24.10 4.20 4 4 4 24.90 3.80 -4 4 -4 23.90 2.90 -4 4 -4 19.30 3.80 -4 4 -4 14.90 2.40 -4 -4 -4 19.10 3.50 -4 -4 -4 20.50 3.50 -4 4 -5 0.80 2.00 4 4 5 0.50 1.60 -4 4 -5 -0.10 2.10 -4 4 -5 1.20 1.40 -4 4 -5 -2.80 1.80 -4 4 -5 1.80 2.30 4 4 5 0.40 1.80 -4 4 -5 0.40 1.10 -4 -4 -5 4.60 2.00 -4 -4 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75.29 5.50 -4 5 8 80.29 3.80 4 5 -8 71.99 6.60 4 -5 -8 80.19 5.70 -4 -5 8 81.89 8.70 4 5 -7 62.59 5.80 -4 5 7 58.79 3.40 -4 5 7 68.09 3.70 -4 5 7 62.49 5.10 4 5 -7 58.99 9.20 -4 -5 7 63.19 6.50 4 -5 -7 57.39 4.90 4 -5 -7 51.99 5.50 -4 5 6 193.98 8.30 4 5 -6 210.88 12.80 -4 5 6 189.38 8.60 -4 5 6 196.68 9.90 -4 5 6 194.38 10.20 4 5 -6 209.88 11.30 4 -5 -6 185.18 10.00 -4 -5 6 209.68 12.00 4 -5 -6 184.28 10.90 -4 5 5 280.57 13.50 4 5 -5 280.87 14.60 -4 5 5 285.97 12.10 4 5 -5 299.07 16.00 -4 5 5 289.37 13.20 -4 5 5 291.27 12.20 4 5 -5 298.97 14.50 -4 -5 5 281.37 14.60 4 -5 -5 291.57 14.30 4 5 -4 183.38 11.60 -4 5 4 186.68 9.40 4 5 -4 169.68 10.30 -4 5 4 164.28 10.00 4 5 -4 181.08 10.30 -4 5 4 172.68 9.70 -4 5 4 170.58 8.60 -4 5 4 186.98 8.30 4 -5 -4 176.88 9.90 -4 -5 4 185.28 10.60 -4 -5 4 170.68 11.30 -4 5 3 2.30 1.80 -4 5 3 4.20 2.00 -4 5 3 6.80 2.50 4 5 -3 1.60 2.00 4 5 -3 2.00 1.90 -4 5 3 1.20 2.10 -4 5 3 3.20 1.50 -4 -5 3 -0.40 2.40 4 -5 -3 4.00 1.90 -4 -5 3 7.80 2.50 4 5 -2 56.29 5.30 4 5 -2 62.69 5.30 -4 5 2 48.10 4.10 -4 5 2 54.39 4.90 4 5 -2 49.70 4.80 -4 5 2 57.79 5.90 -4 5 2 57.59 4.70 -4 5 2 49.30 4.70 -4 -5 2 46.90 6.40 -4 -5 2 55.59 5.00 4 -5 -2 50.59 4.70 4 5 -1 160.48 9.40 -4 5 1 139.39 8.70 -4 5 1 149.69 8.70 -4 5 1 143.09 8.50 4 5 -1 157.48 8.70 -4 5 1 169.38 8.60 -4 5 1 150.98 9.10 4 5 -1 152.88 8.40 4 5 -1 140.79 9.00 4 -5 -1 143.19 8.20 -4 -5 1 148.79 9.90 4 5 0 3.80 1.80 -4 5 0 3.10 2.00 -4 5 0 7.20 2.30 -4 5 0 3.20 2.00 -4 5 0 3.10 1.80 -4 5 0 10.80 2.30 4 5 0 2.60 2.00 -4 5 0 2.40 2.10 4 5 0 6.90 2.10 4 5 0 2.50 1.80 4 -5 0 4.80 1.90 -4 -5 0 6.60 2.60 4 5 1 107.69 5.90 -4 5 -1 92.59 6.60 -4 5 -1 88.89 7.00 4 5 1 98.69 6.80 4 5 1 93.19 6.90 -4 5 -1 93.49 7.00 -4 5 -1 97.49 6.30 4 5 1 93.29 5.80 -4 5 -1 96.69 6.20 -4 5 -1 87.39 6.60 -4 -5 -1 93.79 7.50 -4 -5 -1 88.59 6.90 -4 5 -2 7.70 2.70 -4 5 -2 1.90 1.80 -4 5 -2 7.00 2.40 -4 5 -2 -0.30 1.70 -4 5 -2 5.70 2.00 4 5 2 3.00 2.00 -4 5 -2 2.10 2.20 4 5 2 5.70 1.60 4 5 2 4.90 1.60 -4 -5 -2 4.80 2.50 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4.80 -4 6 7 53.79 3.80 -4 6 7 44.20 3.40 -4 -6 7 58.59 7.30 4 -6 -7 52.09 6.60 -4 6 6 14.10 3.10 4 6 -6 14.80 4.50 -4 6 6 17.40 4.00 -4 6 6 17.90 2.70 -4 6 6 10.20 2.20 4 6 -6 19.10 4.20 -4 -6 6 19.90 4.40 4 -6 -6 13.80 3.50 -4 6 5 41.80 5.40 4 6 -5 42.30 5.90 4 6 -5 42.10 7.10 -4 6 5 49.00 4.30 -4 6 5 38.00 5.10 -4 6 5 41.20 3.50 4 -6 -5 38.20 5.50 -4 -6 5 48.20 6.30 4 6 -4 204.88 11.90 4 6 -4 212.68 13.70 -4 6 4 208.58 10.00 -4 6 4 219.28 11.20 4 6 -4 222.68 12.50 -4 6 4 201.98 11.60 -4 -6 4 212.38 12.20 4 -6 -4 210.48 11.90 -4 6 3 7.20 2.60 4 6 -3 4.10 2.60 4 6 -3 1.70 2.40 4 6 -3 9.80 3.70 -4 6 3 7.20 3.10 -4 6 3 0.40 2.10 -4 6 3 5.90 1.90 -4 -6 3 -0.50 2.90 4 -6 -3 2.70 2.40 -4 6 2 35.70 4.70 -4 6 2 33.90 4.40 4 6 -2 28.00 4.80 4 6 -2 37.10 5.00 4 6 -2 37.90 5.00 -4 6 2 34.40 4.80 4 -6 -2 36.10 5.00 -4 6 1 2.10 2.10 -4 6 1 1.40 2.40 -4 6 1 1.40 2.40 -4 6 1 3.30 1.90 4 6 -1 4.60 2.40 4 6 -1 1.20 2.20 -4 -6 1 4.90 3.00 4 -6 -1 2.80 2.20 -4 6 0 17.90 3.70 -4 6 0 14.10 3.00 4 6 0 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3.70 -4 -7 -6 5.60 4.00 -4 -7 -6 4.10 3.40 5 0 -19 1.40 3.00 5 0 -19 -3.20 3.50 -5 0 19 1.00 3.30 5 0 -18 -0.70 3.30 5 0 -18 0.00 3.20 -5 0 18 -2.50 2.70 -5 0 17 -3.90 2.20 5 0 -17 -1.00 2.60 5 0 -17 -0.50 2.20 5 0 -16 38.00 5.90 5 0 -16 34.00 5.20 -5 0 16 37.60 6.10 5 0 -15 0.50 2.50 5 0 -15 0.50 2.50 5 0 -15 -2.00 1.80 -5 0 15 3.10 2.70 5 0 -14 327.67 16.10 5 0 -14 361.66 17.80 5 0 -14 345.27 16.70 -5 0 14 354.16 17.50 5 0 -13 -2.20 1.70 5 0 -13 3.90 2.10 5 0 -13 0.50 2.00 -5 0 13 0.10 2.10 5 0 -13 2.10 1.90 5 0 -12 191.78 10.50 -5 0 12 191.88 11.20 5 0 -12 215.58 10.80 -5 0 12 204.88 11.30 5 0 -12 200.88 11.50 5 0 -12 200.28 10.90 -5 0 11 -1.20 1.20 5 0 -11 1.40 1.60 5 0 -11 -2.80 1.30 5 0 -11 -1.50 1.10 -5 0 11 -3.30 1.50 5 0 -10 34.70 3.50 5 0 -10 23.00 3.90 -5 0 10 29.00 4.00 5 0 -10 21.00 3.50 -5 0 10 22.50 3.60 5 0 -9 1.20 1.40 -5 0 9 0.00 1.50 5 0 -9 -1.30 1.40 5 0 -9 -0.70 1.30 5 0 -9 0.10 1.20 -5 0 9 1.80 1.70 5 0 -8 113.99 6.50 -5 0 8 103.29 6.70 5 0 -8 107.99 6.70 -5 0 8 102.89 6.30 5 0 -8 99.79 5.90 5 0 -8 89.89 5.60 5 0 -7 0.10 1.00 5 0 -7 -0.70 1.40 5 0 -7 0.10 1.10 -5 0 7 -1.10 0.90 -5 0 7 -1.50 0.70 5 0 -7 -1.60 1.20 5 0 -6 2.90 1.30 -5 0 6 2.00 1.40 5 0 -6 1.80 1.10 5 0 -6 1.00 1.40 -5 0 6 0.50 1.40 5 0 -6 0.60 1.40 5 0 -5 -2.30 1.00 -5 0 5 1.90 1.20 5 0 -5 -1.70 0.80 5 0 -5 -0.40 0.90 -5 0 5 0.90 1.00 -5 0 5 0.30 1.00 5 0 -4 51.19 3.40 -5 0 4 46.70 3.00 5 0 -4 43.30 2.80 -5 0 4 42.60 3.30 -5 0 4 47.90 3.20 5 0 -4 45.80 3.30 -5 0 3 0.30 0.80 5 0 -3 -0.10 0.70 5 0 -3 -0.40 0.80 -5 0 3 -0.50 0.60 5 0 -3 0.70 1.00 -5 0 3 -1.40 0.60 -5 0 2 1.20 0.90 5 0 -2 1.70 0.90 5 0 -2 0.60 0.90 5 0 -2 0.70 0.90 -5 0 2 1.90 0.90 -5 0 2 1.80 0.80 -5 0 1 0.00 0.80 -5 0 1 -0.20 0.80 -5 0 1 -0.30 0.50 5 0 -1 0.30 0.80 5 0 -1 0.70 0.60 5 0 -1 0.20 0.80 -5 0 0 470.85 16.80 5 0 0 501.45 16.80 -5 0 0 494.85 17.60 5 0 0 467.55 17.30 5 0 0 447.86 17.40 -5 0 0 498.95 17.40 5 0 1 -1.00 0.70 5 0 1 -0.20 0.50 -5 0 -1 0.30 1.00 -5 0 -1 1.10 0.80 5 0 1 -0.70 0.60 -5 0 -1 -0.10 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5 -4 5.50 2.40 -5 5 4 6.20 2.50 -5 -5 4 1.40 2.20 -5 -5 4 7.20 3.30 5 -5 -4 3.80 2.00 -5 5 3 86.69 6.40 5 5 -3 93.49 6.80 -5 5 3 86.49 5.60 -5 5 3 78.69 6.50 5 5 -3 100.89 7.10 -5 5 3 92.59 6.60 -5 5 3 93.39 5.40 -5 -5 3 84.79 7.70 -5 -5 3 96.89 6.80 5 -5 -3 101.09 6.70 -5 5 2 50.89 5.00 5 5 -2 48.90 4.80 -5 5 2 63.29 5.20 -5 5 2 55.49 4.20 5 5 -2 49.00 5.00 -5 5 2 47.80 4.40 -5 5 2 52.99 5.30 -5 -5 2 58.89 5.10 -5 -5 2 49.00 6.70 5 -5 -2 45.90 4.60 -5 5 1 17.00 3.40 -5 5 1 15.40 3.40 5 5 -1 22.10 4.60 5 5 -1 18.60 3.30 -5 5 1 18.80 3.80 -5 5 1 21.30 3.40 5 5 -1 26.50 4.50 -5 -5 1 24.30 4.70 -5 -5 1 21.00 3.40 5 -5 -1 19.10 3.20 -5 5 0 36.50 3.90 5 5 0 44.40 5.60 -5 5 0 42.70 4.30 -5 5 0 38.70 4.20 -5 5 0 50.69 4.50 5 5 0 42.60 3.90 5 5 0 48.80 4.80 -5 5 0 49.30 4.90 -5 5 0 50.59 5.00 5 5 0 44.60 4.00 -5 -5 0 43.40 5.90 5 -5 0 41.60 4.00 5 5 1 89.89 5.30 -5 5 -1 75.49 6.40 -5 5 -1 65.39 5.70 5 5 1 76.29 6.40 -5 5 -1 75.69 6.30 -5 5 -1 69.99 5.90 -5 5 -1 75.19 5.50 5 5 1 83.69 6.30 -5 5 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13.80 5 6 -1 48.20 5.80 -5 6 1 46.30 4.80 -5 6 1 49.50 5.20 -5 6 1 52.59 5.40 -5 6 1 54.09 4.80 5 6 -1 43.00 6.00 5 6 -1 48.90 4.80 5 -6 -1 47.70 4.90 -5 6 0 12.30 2.80 -5 6 0 9.10 2.50 -5 6 0 16.10 3.80 5 6 0 15.60 3.50 5 6 0 7.50 2.50 -5 6 0 10.60 3.20 5 6 0 11.60 3.00 -5 6 0 6.00 3.20 -5 -6 0 15.70 4.50 5 6 1 47.90 4.40 5 6 1 47.40 6.30 -5 6 -1 55.09 5.00 -5 6 -1 54.59 5.80 -5 6 -1 52.79 5.50 -5 6 -1 53.29 5.60 -5 6 -1 47.60 4.70 -5 -6 -1 32.40 5.90 5 6 2 486.95 19.50 -5 6 -2 493.55 22.50 -5 6 -2 490.95 20.70 5 6 2 512.55 23.00 -5 6 -2 489.85 22.50 5 6 2 490.95 19.20 -5 -6 -2 521.05 22.90 -5 -6 -2 515.85 23.60 -5 6 -3 64.99 5.80 5 6 3 69.19 4.10 -5 6 -3 66.79 5.50 5 6 3 63.19 3.90 -5 6 -3 70.69 6.70 -5 6 -3 59.99 6.20 -5 -6 -3 71.09 7.00 -5 -6 -3 58.69 6.30 -5 6 -4 31.20 5.80 -5 6 -4 27.10 5.30 -5 6 -4 24.00 3.90 5 6 4 26.60 1.60 -5 6 -4 35.30 4.40 -5 -6 -4 24.30 5.10 -5 -6 -4 29.40 5.10 -5 6 -5 0.40 2.00 -5 6 -5 -3.00 2.70 -5 6 -5 0.70 2.10 -5 6 -5 1.90 2.50 -5 -6 -5 3.20 2.90 -5 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4 -2.50 1.80 -6 -4 -4 1.40 1.50 -6 -4 -4 -0.70 1.70 -6 4 -5 192.68 8.50 6 4 5 174.08 10.10 -6 4 -5 179.48 11.00 -6 4 -5 177.88 8.40 -6 4 -5 196.58 11.20 -6 4 -5 197.78 11.20 -6 -4 -5 192.88 10.70 6 -4 5 198.58 11.40 -6 -4 -5 191.18 10.70 6 4 6 103.89 7.40 -6 4 -6 92.29 7.50 -6 4 -6 107.79 8.00 -6 4 -6 91.39 5.30 -6 4 -6 88.49 5.00 6 -4 6 95.39 7.70 -6 -4 -6 95.29 7.00 -6 -4 -6 90.59 7.10 -6 4 -7 12.60 2.10 6 4 7 8.70 2.60 -6 4 -7 20.50 4.10 -6 4 -7 18.00 4.00 -6 4 -7 18.80 2.70 -6 -4 -7 12.70 3.10 -6 -4 -7 13.60 3.30 -6 4 -8 0.60 1.50 6 4 8 -1.00 2.00 -6 4 -8 0.70 2.40 -6 4 -8 0.30 1.10 -6 -4 -8 1.80 1.90 -6 4 -9 11.90 2.20 -6 4 -9 4.50 2.80 -6 4 -9 9.60 2.60 -6 4 -9 6.10 3.30 -6 -4 -9 8.10 3.10 -6 -4 -9 13.90 3.50 -6 4 -10 35.90 3.90 -6 4 -10 34.80 3.40 -6 4 -10 39.30 6.60 -6 4 -10 39.00 6.10 -6 -4 -10 42.50 5.50 -6 -4 -10 44.40 6.00 -6 4 -11 121.99 7.40 -6 4 -11 125.19 9.70 -6 4 -11 106.19 9.50 6 -4 11 129.69 7.00 -6 -4 -11 116.69 9.10 -6 -4 -11 115.19 8.60 -6 4 -12 66.19 5.30 -6 4 -12 61.69 8.10 -6 4 -12 67.89 8.70 6 -4 12 57.39 4.80 -6 -4 -12 61.79 6.00 -6 -4 -12 52.79 7.20 -6 4 -13 19.60 3.60 -6 4 -13 19.70 5.00 -6 4 -13 20.70 6.30 -6 -4 -13 21.10 4.50 6 -4 13 18.50 3.50 -6 -4 -13 17.30 4.70 -6 4 -14 4.20 4.30 -6 4 -14 0.00 2.20 -6 -4 -14 3.40 2.70 6 -4 14 0.10 3.30 -6 -4 -14 0.30 2.70 6 5 -14 65.59 10.10 6 5 -14 60.59 8.70 -6 5 14 57.39 5.70 6 -5 -14 67.99 10.30 -6 -5 14 60.69 10.40 -6 5 13 2.30 2.20 6 5 -13 2.60 3.80 6 5 -13 1.30 3.20 6 -5 -13 5.40 3.50 6 -5 -13 1.30 3.10 -6 -5 13 -5.10 3.30 -6 5 12 9.60 3.10 6 5 -12 17.20 4.50 6 5 -12 11.90 4.80 6 -5 -12 19.60 4.30 -6 -5 12 21.20 5.10 6 -5 -12 17.50 3.60 -6 5 11 -0.60 1.80 6 5 -11 -0.90 2.60 6 5 -11 -1.70 3.20 6 -5 -11 -1.10 2.40 -6 -5 11 -2.40 2.40 6 -5 -11 -0.10 2.10 -6 5 10 35.80 5.00 6 5 -10 40.70 6.10 6 5 -10 45.80 7.00 6 -5 -10 46.10 4.90 6 -5 -10 48.40 6.60 -6 -5 10 42.20 7.20 -6 5 9 250.57 12.40 6 5 -9 238.08 15.00 6 5 -9 252.27 13.90 6 -5 -9 243.78 13.70 6 -5 -9 242.08 12.40 -6 -5 9 237.38 14.40 -6 5 8 79.59 6.00 6 5 -8 72.49 6.70 6 5 -8 75.99 7.60 -6 -5 8 71.89 9.60 6 -5 -8 70.99 6.50 6 -5 -8 66.89 5.90 6 5 -7 72.49 7.70 -6 5 7 91.79 6.30 6 5 -7 81.19 8.00 6 -5 -7 67.19 6.20 -6 -5 7 87.09 7.40 6 -5 -7 78.49 6.20 -6 5 6 0.80 0.50 6 5 -6 2.60 2.20 -6 5 6 1.00 2.00 6 -5 -6 8.90 2.60 6 -5 -6 1.80 1.90 -6 -5 6 -0.10 1.80 -6 5 5 20.50 3.80 -6 5 5 21.20 1.90 6 5 -5 14.80 3.40 -6 5 5 18.10 2.00 -6 5 5 22.60 3.80 6 5 -5 16.20 3.40 6 -5 -5 22.30 3.80 -6 -5 5 23.50 4.20 -6 -5 5 21.70 4.80 6 -5 -5 21.00 3.80 -6 5 4 268.07 12.80 -6 5 4 271.77 13.40 6 5 -4 234.08 13.00 -6 5 4 259.87 11.00 6 5 -4 272.47 13.70 -6 5 4 247.38 13.10 -6 5 4 260.67 10.70 -6 -5 4 281.07 13.60 6 -5 -4 261.37 13.30 6 -5 -4 263.57 12.80 -6 -5 4 258.97 15.00 -6 5 3 173.88 9.80 -6 5 3 171.38 11.10 -6 5 3 178.48 8.40 6 5 -3 176.48 10.10 6 5 -3 187.28 10.60 -6 5 3 177.38 8.70 -6 5 3 181.48 10.40 6 -5 -3 184.68 9.70 -6 -5 3 200.08 10.50 -6 -5 3 183.48 11.70 -6 5 2 142.99 8.50 -6 5 2 139.59 8.60 6 5 -2 140.99 9.10 6 5 -2 136.59 8.20 -6 5 2 143.59 7.80 -6 5 2 139.09 7.50 -6 5 2 140.49 8.90 -6 -5 2 121.39 9.40 6 -5 -2 141.89 8.10 -6 -5 2 158.88 8.60 -6 5 1 0.40 1.90 -6 5 1 3.70 2.20 -6 5 1 5.40 2.10 -6 5 1 0.60 2.00 -6 5 1 1.90 2.10 6 5 -1 3.40 1.80 6 5 -1 8.70 3.00 -6 -5 1 -0.20 2.40 -6 -5 1 4.30 1.70 6 -5 -1 5.70 1.90 6 5 0 309.27 13.10 6 5 0 306.17 15.10 -6 5 0 304.57 13.30 -6 5 0 283.77 13.40 -6 5 0 306.57 14.80 -6 5 0 303.77 14.10 6 5 0 298.47 13.10 -6 5 0 311.37 14.00 6 -5 0 296.87 13.10 -6 -5 0 287.47 15.60 6 5 1 230.28 10.60 6 5 1 250.37 10.60 6 5 1 239.48 12.90 -6 5 -1 254.17 13.00 -6 5 -1 233.68 12.30 -6 5 -1 254.07 12.50 -6 5 -1 255.57 11.60 -6 5 -1 242.38 11.10 -6 -5 -1 239.38 12.80 -6 -5 -1 236.58 13.30 -6 5 -2 21.90 3.10 -6 5 -2 13.50 2.60 -6 5 -2 11.30 3.50 -6 5 -2 17.00 3.60 6 5 2 16.90 2.20 6 5 2 17.70 2.20 -6 -5 -2 12.40 3.20 -6 -5 -2 18.50 4.20 6 5 3 62.59 3.10 -6 5 -3 60.19 6.00 -6 5 -3 52.49 5.60 -6 5 -3 59.69 4.50 -6 5 -3 57.49 5.70 -6 5 -3 57.79 4.80 6 5 3 60.19 3.00 -6 -5 -3 69.59 6.40 -6 -5 -3 61.69 6.00 -6 5 -4 30.60 5.00 -6 5 -4 35.30 5.90 -6 5 -4 40.00 5.80 -6 5 -4 39.20 3.70 -6 -5 -4 42.00 5.80 -6 -5 -4 41.70 5.70 -6 5 -5 183.48 8.90 -6 5 -5 176.68 11.30 -6 5 -5 175.18 11.10 -6 -5 -5 169.48 10.90 -6 -5 -5 190.18 11.20 -6 5 -6 22.90 3.10 -6 5 -6 16.10 3.40 -6 5 -6 17.70 4.10 -6 5 -6 10.80 3.70 -6 -5 -6 19.80 4.20 -6 -5 -6 15.30 4.20 -6 5 -7 9.70 3.30 -6 5 -7 5.10 3.50 -6 5 -7 6.10 2.10 -6 5 -7 6.60 2.20 -6 -5 -7 7.50 3.20 -6 -5 -7 5.70 2.60 -6 5 -8 28.30 3.70 -6 5 -8 30.50 5.40 -6 5 -8 28.30 3.60 -6 5 -8 43.40 6.50 -6 -5 -8 34.50 5.40 -6 -5 -8 28.90 5.10 -6 5 -9 -0.50 1.70 -6 5 -9 3.80 1.80 -6 5 -9 -1.10 1.90 -6 5 -9 -2.40 1.70 -6 -5 -9 0.10 2.50 -6 -5 -9 2.50 2.50 -6 5 -10 37.20 4.00 -6 5 -10 46.80 4.50 -6 5 -10 44.40 7.30 -6 5 -10 42.60 7.00 -6 -5 -10 40.30 6.00 -6 -5 -10 45.10 6.50 -6 5 -11 1.40 2.50 -6 5 -11 5.00 4.20 -6 5 -11 2.10 4.40 -6 -5 -11 0.10 2.60 -6 -5 -11 -1.10 2.80 -6 5 -12 10.30 4.90 -6 5 -12 5.10 2.90 -6 -5 -12 10.70 3.80 -6 5 -13 -2.30 3.80 -6 5 -13 9.00 3.00 -6 5 -13 2.80 4.70 -6 -5 -13 0.90 3.40 -6 -5 -13 -3.30 2.80 6 6 -11 48.70 8.70 -6 6 11 57.89 5.50 6 6 -11 52.29 7.60 6 -6 -11 42.30 7.00 -6 -6 11 54.29 8.30 6 6 -10 4.70 3.60 6 6 -10 0.90 2.90 -6 6 10 4.70 2.40 -6 -6 10 -3.40 2.40 6 -6 -10 2.10 3.10 6 6 -9 17.70 5.30 6 6 -9 16.00 4.30 -6 6 9 24.10 4.00 6 -6 -9 22.50 4.80 -6 -6 9 14.80 4.50 6 6 -8 209.28 14.50 6 6 -8 188.58 12.50 -6 6 8 206.58 11.30 6 -6 -8 212.98 12.60 -6 -6 8 219.18 13.80 6 6 -7 31.90 6.70 6 6 -7 32.70 5.60 -6 6 7 27.00 4.40 6 -6 -7 27.50 5.40 -6 -6 7 42.20 6.30 6 6 -6 3.40 3.00 -6 6 6 3.50 2.20 6 6 -6 9.10 4.10 -6 6 6 2.20 1.10 -6 6 6 1.50 1.10 6 -6 -6 8.00 2.60 -6 -6 6 3.90 3.00 6 6 -5 9.40 3.80 -6 6 5 9.90 2.10 -6 6 5 12.10 3.10 6 6 -5 9.90 3.40 6 -6 -5 22.30 4.40 -6 -6 5 15.00 4.20 -6 -6 5 4.60 3.70 -6 6 4 6.20 2.70 -6 6 4 -1.50 1.70 -6 6 4 3.80 1.40 6 6 -4 0.90 2.20 -6 -6 4 2.80 2.60 6 -6 -4 3.00 2.40 -6 -6 4 4.00 2.80 -6 6 3 1.70 1.60 6 6 -3 -0.90 2.40 6 6 -3 3.40 2.10 -6 6 3 2.90 2.40 -6 6 3 2.50 2.20 6 -6 -3 3.70 2.00 -6 -6 3 1.20 2.70 -6 -6 3 4.40 2.40 6 6 -2 -5.00 1.70 6 6 -2 -3.30 2.20 6 6 -2 0.70 2.50 -6 6 2 1.10 1.70 -6 6 2 -0.70 1.70 -6 6 2 0.60 2.10 6 -6 -2 0.40 1.60 -6 -6 2 -0.60 2.80 -6 6 1 6.80 2.00 -6 6 1 4.60 2.60 -6 6 1 5.00 2.30 -6 6 1 1.90 2.60 -6 6 1 6.60 2.70 6 6 -1 5.20 2.40 6 6 -1 5.30 2.40 6 6 -1 3.00 2.30 6 -6 -1 5.10 2.10 -6 -6 1 4.10 3.20 -6 6 0 70.49 5.60 6 6 0 72.19 5.30 6 6 0 70.29 5.20 -6 6 0 69.99 6.00 6 6 0 68.09 6.60 -6 6 0 76.79 6.10 -6 6 0 61.99 5.90 -6 -6 0 70.09 8.60 -6 6 -1 67.49 6.00 6 6 1 61.49 4.50 -6 6 -1 55.59 5.10 -6 6 -1 68.39 6.40 -6 6 -1 69.09 6.20 -6 6 -1 58.19 5.60 6 6 1 63.29 6.40 6 6 1 58.49 4.60 -6 6 -2 36.80 5.70 6 6 2 46.30 6.40 -6 6 -2 51.59 5.00 6 6 2 52.19 3.80 6 6 2 47.20 3.50 -6 6 -2 39.80 4.80 -6 6 -2 50.59 6.40 -6 -6 -2 45.70 6.30 -6 6 -3 0.80 2.20 6 6 3 4.00 1.20 -6 6 -3 10.10 3.40 -6 6 -3 2.20 3.00 -6 6 -3 5.10 2.20 6 6 3 7.40 1.30 -6 -6 -3 5.30 2.70 -6 6 -4 55.29 7.00 -6 6 -4 38.20 6.20 -6 6 -4 42.20 4.20 -6 -6 -4 31.50 5.40 -6 -6 -4 64.79 8.70 -6 6 -5 63.79 5.40 -6 6 -5 75.99 7.40 -6 6 -5 73.59 7.30 -6 -6 -5 61.29 7.70 -6 6 -6 14.20 3.00 -6 6 -6 25.50 5.70 -6 6 -6 13.30 4.30 -6 -6 -6 27.00 5.20 -6 6 -7 16.70 3.20 -6 6 -7 11.60 4.30 -6 6 -7 13.80 4.40 -6 -6 -7 17.00 4.90 -6 -6 -7 16.50 4.40 -6 6 -8 96.19 9.10 -6 6 -8 80.69 6.10 -6 6 -8 80.39 8.40 -6 6 -8 67.99 5.80 -6 -6 -8 82.69 8.10 -6 -6 -8 87.29 8.10 -6 6 -9 10.20 4.70 -6 6 -9 7.50 2.90 -6 -6 -9 13.30 4.10 -6 -6 -9 11.00 3.60 -6 6 -10 61.99 5.80 -6 6 -10 46.30 8.00 -6 -6 -10 57.09 7.50 -6 -6 -10 52.89 7.60 6 7 -6 6.70 4.90 6 7 -6 8.20 3.60 6 7 -6 9.10 3.80 -6 7 6 1.30 2.80 6 -7 -6 7.50 3.80 -6 -7 6 2.00 3.90 6 7 -5 12.80 4.70 -6 7 5 5.10 2.20 6 7 -5 14.00 3.40 6 7 -5 8.90 3.80 -6 7 5 2.90 3.00 6 -7 -5 9.10 3.40 6 7 -4 1.30 3.00 -6 7 4 4.90 3.30 6 7 -4 -0.70 3.50 6 7 -4 6.70 3.20 6 -7 -4 3.80 2.70 6 7 -3 2.70 2.90 6 7 -3 5.80 3.40 -6 7 3 6.90 3.00 -6 7 3 0.60 2.40 -6 7 3 4.90 2.90 6 7 -3 7.90 4.20 -6 -7 3 5.90 4.30 6 -7 -3 8.50 3.10 -6 7 2 6.20 2.90 6 7 -2 6.50 2.90 -6 7 2 2.30 2.20 -6 7 2 7.00 2.60 6 7 -2 7.80 4.10 -6 7 2 0.00 2.70 6 7 -2 7.60 3.60 -6 -7 2 10.10 4.70 -6 7 1 57.09 6.00 6 7 -1 62.89 5.40 6 7 -1 73.99 6.20 -6 7 1 71.99 6.90 -6 7 1 44.10 5.70 6 7 -1 56.19 7.50 -6 7 1 55.29 5.70 -6 -7 1 56.29 8.20 6 7 0 9.50 2.70 6 7 0 9.70 4.00 -6 7 0 4.80 3.10 -6 7 0 7.90 3.30 -6 -7 0 12.50 4.90 6 7 1 38.50 4.30 -6 7 -1 35.90 4.80 -6 7 -1 37.10 6.00 6 7 1 36.20 5.30 6 7 1 30.40 5.70 -6 7 -1 46.20 6.30 -6 -7 -1 34.90 6.50 -6 7 -2 19.10 4.30 -6 7 -2 34.20 6.00 6 7 2 28.40 3.30 6 7 2 30.00 6.10 -6 7 -2 27.60 4.30 -6 -7 -2 37.10 6.40 -6 7 -3 20.10 4.50 -6 7 -3 19.90 5.60 -6 7 -3 19.80 4.00 6 7 3 25.00 2.00 -6 -7 -3 35.90 6.40 -6 7 -4 -0.80 3.00 -6 7 -4 -1.50 2.30 -6 7 -4 -1.80 3.40 6 7 4 -1.40 3.20 -6 -7 -4 -5.10 3.20 -6 -7 -4 2.50 3.00 -6 7 -5 17.70 4.90 -6 7 -5 22.80 3.80 -6 7 -5 13.60 5.30 -6 -7 -5 13.90 5.00 -6 -7 -5 23.60 4.90 7 0 -19 5.80 5.50 7 0 -19 1.20 3.00 -7 0 19 5.80 4.10 7 0 -18 156.48 12.30 -7 0 18 169.68 12.60 7 0 -18 191.78 11.80 7 0 -17 2.90 3.10 -7 0 17 1.00 2.70 7 0 -17 0.50 2.80 7 0 -16 25.90 5.30 7 0 -16 22.40 4.20 -7 0 16 13.30 4.10 7 0 -16 20.30 4.50 7 0 -15 2.10 2.20 7 0 -15 1.80 1.90 7 0 -15 -2.90 2.30 7 0 -14 208.28 12.40 -7 0 14 164.18 11.20 7 0 -14 182.18 10.40 -7 0 13 0.70 1.50 7 0 -13 2.20 2.10 7 0 -13 0.40 1.70 7 0 -13 0.00 2.30 7 0 -12 123.39 7.50 7 0 -12 107.09 7.50 7 0 -12 95.49 7.60 7 0 -12 106.09 7.00 -7 0 12 103.49 7.90 7 0 -11 -0.20 1.70 7 0 -11 -0.60 1.70 7 0 -11 -0.90 1.50 7 0 -11 -1.80 1.70 -7 0 11 -2.90 1.50 -7 0 11 -0.60 1.10 7 0 -10 231.38 11.20 7 0 -10 237.08 11.40 -7 0 10 233.28 12.40 7 0 -10 255.17 12.30 7 0 -10 240.28 12.50 -7 0 10 265.17 13.80 7 0 -9 3.10 2.00 7 0 -9 -0.70 1.30 -7 0 9 3.30 2.00 7 0 -9 0.00 1.40 -7 0 9 -1.60 1.30 7 0 -9 -1.20 1.30 -7 0 8 6.50 1.60 7 0 -8 5.50 1.90 -7 0 8 7.00 2.30 7 0 -8 12.20 2.60 7 0 -8 5.90 2.40 7 0 -8 7.20 2.00 -7 0 7 0.40 1.40 7 0 -7 -0.20 1.40 -7 0 7 0.60 1.40 7 0 -7 0.80 1.30 7 0 -7 2.50 2.20 7 0 -7 1.00 1.20 7 0 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930.61 32.00 -10 -2 5 993.30 35.60 -10 2 4 76.59 4.00 10 2 -4 79.99 5.70 10 2 -4 81.79 5.80 -10 2 4 77.79 5.80 -10 2 4 88.59 5.10 10 2 -4 81.89 5.50 -10 -2 4 92.39 5.70 -10 -2 4 76.99 5.70 10 -2 -4 88.79 4.30 10 -2 -4 84.29 5.10 10 -2 -4 85.69 5.70 -10 -2 4 105.19 6.70 10 2 -3 16.80 2.90 10 2 -3 17.80 3.00 10 2 -3 14.20 2.50 -10 2 3 15.70 2.90 10 2 -3 10.70 2.60 -10 2 3 13.10 1.80 -10 2 3 15.30 2.20 10 -2 -3 14.00 2.80 -10 -2 3 11.10 2.70 10 -2 -3 14.40 2.20 -10 -2 3 15.00 3.10 -10 -2 3 14.80 2.40 10 -2 -3 15.50 2.00 10 2 -2 135.99 7.30 10 2 -2 129.69 6.90 -10 2 2 132.09 6.40 -10 2 2 137.69 7.80 10 2 -2 116.89 7.50 10 2 -2 148.69 7.60 -10 2 2 133.39 6.00 10 -2 -2 137.29 7.70 10 -2 -2 123.59 6.50 -10 -2 2 136.49 8.00 -10 -2 2 126.29 7.20 10 -2 -2 141.79 6.20 10 2 -1 328.67 14.20 10 2 -1 364.56 15.20 -10 2 1 363.46 15.60 -10 2 1 365.96 14.40 10 2 -1 387.46 16.00 10 2 -1 370.46 15.20 -10 2 1 354.56 13.00 -10 -2 1 365.76 14.80 10 -2 -1 342.67 13.10 10 -2 -1 361.96 14.70 10 -2 -1 361.66 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82.19 6.40 -10 -2 -4 81.59 6.20 10 2 5 38.80 4.70 -10 2 -5 42.80 4.40 -10 2 -5 37.60 5.00 10 2 5 42.50 5.40 -10 2 -5 38.70 5.20 -10 -2 -5 42.80 2.80 -10 -2 -5 36.30 4.90 -10 -2 -5 36.30 2.60 10 -2 5 41.70 5.60 -10 -2 -5 44.80 4.10 -10 2 -6 144.99 9.40 10 2 6 158.38 9.50 -10 2 -6 166.28 9.80 -10 2 -6 158.78 9.30 10 2 6 141.49 8.50 -10 -2 -6 146.79 9.30 -10 -2 -6 149.09 8.40 -10 -2 -6 154.38 6.60 10 -2 6 136.49 9.50 -10 -2 -6 155.08 6.40 -10 2 -7 657.93 28.00 10 2 7 681.83 27.30 -10 2 -7 647.04 27.90 -10 2 -7 634.64 27.30 10 -2 7 673.73 23.00 -10 -2 -7 707.93 24.10 -10 -2 -7 696.23 23.80 -10 -2 -7 643.34 27.60 -10 -2 -7 698.93 26.70 -10 2 -8 22.30 1.80 10 2 8 28.30 4.50 -10 2 -8 28.60 4.80 -10 2 -8 20.90 4.10 -10 -2 -8 27.20 4.20 10 -2 8 28.30 1.90 -10 -2 -8 22.80 2.20 -10 -2 -8 23.60 2.10 -10 -2 -8 24.20 4.30 -10 2 -9 79.59 4.20 10 2 9 76.49 6.70 -10 2 -9 86.49 7.40 -10 2 -9 77.99 6.60 -10 -2 -9 90.19 7.10 -10 -2 -9 75.29 4.10 -10 -2 -9 80.79 6.20 -10 -2 -9 83.69 4.40 10 -2 9 81.89 4.20 -10 2 -10 22.50 4.60 -10 2 -10 28.00 2.60 -10 2 -10 27.60 4.90 -10 -2 -10 30.70 2.40 -10 -2 -10 27.80 4.70 -10 -2 -10 24.50 2.50 -10 2 -11 -1.50 2.60 -10 2 -11 1.50 2.20 -10 2 -11 0.40 1.40 -10 -2 -11 0.60 2.20 -10 -2 -11 0.70 1.10 -10 -2 -11 0.30 1.20 -10 -2 -11 0.70 1.90 10 -2 11 0.10 1.40 -10 2 -12 27.60 5.50 -10 2 -12 17.70 4.50 -10 2 -12 28.60 3.40 -10 -2 -12 21.90 2.50 10 -2 12 19.70 3.00 -10 -2 -12 22.40 3.70 -10 -2 -12 22.90 5.20 -10 2 -13 112.89 9.00 -10 2 -13 99.49 9.60 -10 2 -13 106.19 6.60 -10 -2 -13 123.59 8.70 10 -2 13 112.39 6.80 -10 -2 -13 127.69 9.50 -10 -2 -13 111.39 5.70 -10 2 -14 18.20 4.60 -10 2 -14 15.90 3.00 -10 2 -14 11.00 4.50 -10 -2 -14 9.60 4.30 10 -2 14 12.10 3.50 -10 -2 -14 17.00 2.50 -10 -2 -14 20.90 4.40 -10 -2 -14 17.70 3.20 -10 2 -15 4.30 4.00 -10 2 -15 17.20 3.50 -10 2 -15 15.50 4.20 -10 -2 -15 8.80 2.50 -10 -2 -15 14.00 4.00 -10 -2 -15 9.30 4.40 10 3 -17 18.40 5.80 -10 3 17 40.50 6.50 10 3 -17 28.70 6.60 10 -3 -17 34.30 6.80 -10 -3 17 29.70 6.80 10 3 -16 33.00 6.90 -10 3 16 47.60 6.80 10 3 -16 31.90 6.30 10 -3 -16 35.00 6.60 -10 -3 16 45.50 8.00 -10 3 15 27.20 5.40 10 3 -15 23.20 5.40 10 3 -15 22.10 5.70 10 -3 -15 29.70 5.40 -10 -3 15 27.80 6.00 10 3 -14 99.69 8.90 10 3 -14 91.29 8.80 -10 3 14 81.79 7.40 10 -3 -14 88.09 8.10 -10 -3 14 64.69 9.10 10 3 -13 98.69 8.60 10 3 -13 85.59 8.80 -10 3 13 90.89 7.80 10 -3 -13 97.79 8.30 -10 -3 13 92.69 9.00 10 3 -12 32.60 5.50 10 3 -12 32.80 5.90 -10 3 12 24.80 4.80 -10 -3 12 24.60 5.30 10 -3 -12 23.20 4.60 10 3 -11 2.70 3.00 10 3 -11 1.20 2.10 -10 3 11 1.90 2.20 10 -3 -11 2.20 2.50 -10 -3 11 3.20 2.70 10 3 -10 79.79 7.10 10 3 -10 75.29 7.40 -10 3 10 75.09 6.30 10 -3 -10 65.39 6.20 -10 -3 10 75.39 7.40 -10 -3 10 68.29 7.10 -10 3 9 26.90 4.50 10 3 -9 25.30 4.70 -10 3 9 26.30 4.40 10 -3 -9 24.90 4.10 10 -3 -9 22.10 4.40 -10 -3 9 31.20 5.30 -10 -3 9 23.30 4.60 10 3 -8 64.09 5.80 -10 3 8 41.70 5.30 -10 3 8 48.70 5.10 10 3 -8 46.30 4.80 -10 -3 8 46.60 6.30 -10 -3 8 54.49 6.70 10 -3 -8 51.29 4.80 10 -3 -8 45.40 5.70 -10 3 7 205.88 10.70 -10 3 7 208.58 11.10 10 3 -7 199.48 11.20 10 3 -7 200.28 11.10 10 -3 -7 222.88 10.90 -10 -3 7 191.68 11.80 10 -3 -7 202.58 10.70 -10 -3 7 179.08 11.20 10 3 -6 10.00 2.70 10 3 -6 6.40 2.00 -10 3 6 7.40 2.40 10 3 -6 9.90 2.60 -10 3 6 10.00 2.90 -10 -3 6 8.80 3.10 -10 -3 6 10.30 3.00 -10 -3 6 8.00 2.40 10 -3 -6 5.40 2.30 10 -3 -6 6.40 2.20 10 3 -5 72.79 5.80 -10 3 5 65.19 5.10 -10 3 5 73.49 5.70 10 3 -5 74.19 5.50 10 3 -5 61.39 5.60 10 3 -5 60.59 5.30 -10 -3 5 64.29 5.10 -10 -3 5 68.99 5.80 -10 -3 5 77.89 6.50 10 -3 -5 68.69 5.90 10 -3 -5 73.59 5.70 10 3 -4 17.40 3.00 10 3 -4 16.40 2.90 -10 3 4 13.80 2.50 -10 3 4 12.50 3.00 -10 3 4 13.20 1.30 10 3 -4 9.40 2.80 10 3 -4 19.10 3.50 10 -3 -4 15.30 2.60 -10 -3 4 12.60 3.40 10 -3 -4 14.30 3.00 -10 -3 4 14.10 3.20 10 3 -3 197.88 9.70 -10 3 3 201.48 10.60 10 3 -3 189.58 10.20 -10 3 3 193.78 9.00 10 3 -3 207.58 10.50 -10 3 3 189.58 8.20 10 3 -3 196.08 10.70 10 -3 -3 186.08 8.40 10 -3 -3 209.88 9.00 -10 -3 3 203.38 10.40 10 -3 -3 213.48 10.80 -10 -3 3 194.68 11.20 10 3 -2 91.99 5.80 10 3 -2 98.39 7.00 10 3 -2 94.19 6.40 -10 3 2 99.69 7.00 -10 3 2 100.69 5.40 -10 3 2 105.29 5.40 10 3 -2 112.89 7.00 10 -3 -2 99.49 5.60 -10 -3 2 102.29 6.40 10 -3 -2 111.29 5.30 -10 -3 2 90.29 7.20 10 -3 -2 88.69 6.60 -10 3 1 611.44 20.70 10 3 -1 572.84 21.60 -10 3 1 580.34 21.60 10 3 -1 537.45 23.40 10 3 -1 587.94 23.20 -10 3 1 548.35 23.20 10 3 -1 570.24 23.10 -10 -3 1 548.95 22.10 10 -3 -1 580.64 22.10 10 -3 -1 576.84 23.70 10 -3 -1 539.65 20.40 -10 -3 1 573.24 24.20 10 3 0 62.19 5.00 -10 3 0 50.89 2.70 -10 3 0 58.69 4.40 10 3 0 55.09 3.70 -10 3 0 53.59 5.10 10 3 0 55.39 5.00 10 3 0 49.10 4.70 -10 -3 0 48.50 3.90 10 -3 0 53.99 4.40 10 -3 0 50.79 2.60 -10 -3 0 47.60 5.20 10 -3 0 52.49 5.00 10 3 1 163.78 7.20 10 3 1 164.98 9.20 10 3 1 153.48 8.90 10 3 1 157.38 9.20 -10 3 -1 159.48 9.30 10 -3 1 179.68 9.10 10 -3 1 154.28 9.30 -10 -3 -1 150.18 7.40 -10 -3 -1 154.78 9.60 10 3 2 26.40 2.20 -10 3 -2 35.40 4.40 10 3 2 24.60 4.10 10 3 2 24.00 3.60 -10 3 -2 27.70 4.30 -10 3 -2 23.50 4.40 10 3 2 26.50 4.10 -10 -3 -2 26.00 4.30 10 -3 2 17.50 3.80 -10 -3 -2 33.00 4.30 -10 -3 -2 27.80 2.40 10 -3 2 32.20 4.40 -10 3 -3 25.30 4.40 -10 3 -3 24.30 3.90 10 3 3 24.30 1.80 -10 3 -3 21.90 3.90 10 3 3 14.30 3.60 10 3 3 24.30 4.00 -10 -3 -3 24.10 4.50 10 -3 3 24.50 3.90 -10 -3 -3 20.00 3.70 -10 -3 -3 25.30 1.90 10 3 4 43.10 4.50 10 3 4 45.40 5.50 -10 3 -4 48.60 5.10 -10 3 -4 50.79 5.20 10 -3 4 45.50 6.80 -10 -3 -4 47.50 5.30 -10 -3 -4 43.80 4.50 10 3 5 314.87 15.20 -10 3 -5 317.67 15.40 -10 3 -5 306.57 15.50 -10 -3 -5 333.47 15.00 10 -3 5 296.87 15.60 -10 -3 -5 315.97 15.60 -10 3 -6 3.50 2.60 -10 3 -6 6.20 2.80 -10 -3 -6 9.50 2.80 -10 -3 -6 1.80 1.80 -10 3 -7 104.19 8.10 -10 3 -7 106.09 8.10 -10 -3 -7 88.69 7.00 -10 -3 -7 100.69 7.80 -10 3 -8 191.88 12.00 -10 -3 -8 191.18 11.00 -10 -3 -8 191.48 11.60 -10 3 -9 191.08 12.10 -10 3 -9 208.78 12.20 -10 3 -9 187.28 7.30 -10 3 -9 192.58 7.30 -10 -3 -9 192.78 11.20 -10 3 -10 2.10 1.00 -10 3 -10 5.60 2.80 -10 3 -10 3.60 3.00 -10 -3 -10 4.50 2.40 -10 -3 -10 3.40 2.50 -10 3 -11 34.40 5.90 -10 3 -11 35.70 5.90 -10 3 -11 30.70 2.70 -10 -3 -11 37.30 5.80 -10 -3 -11 28.50 4.90 -10 3 -12 17.50 4.40 -10 3 -12 15.60 2.30 -10 3 -12 18.30 5.30 -10 -3 -12 12.90 4.10 -10 -3 -12 12.90 3.50 10 -3 12 15.50 2.40 -10 3 -13 -6.90 2.60 -10 3 -13 -0.60 1.80 -10 3 -13 3.50 3.70 -10 -3 -13 2.40 2.80 -10 -3 -13 1.50 3.40 10 -3 13 -1.30 2.10 -10 3 -14 6.00 4.10 -10 3 -14 -1.10 4.00 -10 3 -14 2.00 2.00 -10 -3 -14 3.80 3.80 -10 -3 -14 2.10 3.40 10 4 -15 43.90 8.20 -10 4 15 45.50 6.80 10 4 -15 65.59 10.40 10 -4 -15 66.79 8.90 -10 4 14 -1.80 2.30 10 4 -14 -1.70 2.80 10 4 -14 3.90 3.50 10 -4 -14 -0.60 3.00 -10 -4 14 -0.80 3.20 10 4 -13 11.60 4.50 10 4 -13 0.70 3.20 -10 4 13 2.20 2.90 -10 -4 13 5.10 3.80 10 -4 -13 2.30 3.00 -10 4 12 96.49 8.10 10 4 -12 73.39 7.80 10 4 -12 76.49 8.60 10 -4 -12 95.59 8.20 -10 -4 12 106.89 9.30 10 4 -11 78.09 8.40 10 4 -11 76.99 7.60 -10 4 11 79.59 7.00 -10 -4 11 74.79 8.00 10 -4 -11 80.59 7.40 10 4 -10 170.58 12.40 -10 4 10 179.48 10.90 10 4 -10 183.78 11.70 10 -4 -10 178.88 11.10 -10 -4 10 183.98 12.20 -10 4 9 127.49 8.80 10 4 -9 151.58 11.00 10 4 -9 139.39 9.70 -10 -4 9 115.99 9.90 10 -4 -9 154.08 9.50 -10 -4 9 127.29 9.90 10 4 -8 19.50 4.00 -10 4 8 16.10 3.20 -10 4 8 14.10 3.50 -10 -4 8 10.90 4.10 -10 -4 8 24.70 5.00 10 -4 -8 21.10 3.70 10 4 -7 111.39 9.80 -10 4 7 135.09 8.50 -10 4 7 110.69 8.00 -10 -4 7 129.29 9.20 -10 -4 7 136.49 11.50 10 -4 -7 138.69 8.30 -10 4 6 223.48 12.10 10 4 -6 232.58 12.30 10 4 -6 242.68 12.80 -10 4 6 205.38 11.60 10 -4 -6 230.38 11.50 -10 -4 6 229.58 13.90 -10 -4 6 224.38 12.60 -10 4 5 23.60 3.90 10 4 -5 16.20 3.80 10 4 -5 20.50 3.50 -10 4 5 20.20 3.40 -10 -4 5 25.50 4.20 10 -4 -5 18.10 3.30 -10 -4 5 15.60 4.50 -10 4 4 374.86 13.70 10 4 -4 347.47 17.30 -10 4 4 408.06 17.70 -10 4 4 379.76 16.20 10 4 -4 370.76 16.70 -10 4 4 396.56 13.60 10 -4 -4 380.96 15.90 -10 -4 4 332.07 18.30 -10 -4 4 396.76 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15.50 1.50 -10 -4 -2 8.70 3.20 -10 -4 -2 16.80 2.00 -10 -4 -2 14.20 3.40 10 -4 2 19.60 4.00 -10 4 -3 26.00 4.40 -10 4 -3 24.00 4.80 -10 -4 -3 18.50 3.80 10 -4 3 30.00 4.60 -10 -4 -3 23.70 4.80 -10 4 -4 5.30 2.40 -10 4 -4 -0.30 2.20 10 -4 4 6.60 2.90 -10 -4 -4 5.80 2.80 -10 -4 -4 1.90 2.50 -10 4 -5 0.70 2.00 -10 4 -5 6.70 2.50 -10 -4 -5 4.10 2.90 -10 -4 -5 2.20 2.10 -10 4 -6 28.60 5.00 -10 4 -6 38.90 5.60 -10 -4 -6 32.50 5.00 -10 -4 -6 27.80 5.00 -10 4 -7 164.28 11.10 -10 -4 -7 163.48 10.40 -10 4 -8 16.20 3.90 -10 4 -8 22.50 5.10 -10 -4 -8 20.70 4.20 -10 -4 -8 30.40 5.40 -10 4 -9 -0.50 2.40 -10 4 -9 6.90 3.10 -10 -4 -9 6.00 2.60 -10 -4 -9 11.30 3.90 -10 4 -10 38.70 6.90 -10 4 -10 30.50 1.80 -10 4 -10 37.20 6.40 -10 -4 -10 32.40 5.40 -10 -4 -10 32.80 5.40 -10 4 -11 26.80 2.10 -10 4 -11 35.70 7.00 -10 4 -11 26.50 2.10 -10 4 -11 25.60 5.70 -10 -4 -11 26.30 5.50 -10 -4 -11 23.40 5.00 -10 4 -12 3.80 1.40 -10 4 -12 4.30 4.20 -10 4 -12 -3.00 3.50 -10 -4 -12 1.10 3.80 -10 -4 -12 4.20 3.20 -10 4 -13 2.60 3.90 -10 4 -13 -1.70 3.20 -10 -4 -13 6.20 3.90 -10 -4 -13 2.50 3.20 -10 5 13 1.60 3.20 10 5 -13 -4.20 4.10 -10 -5 13 3.10 3.80 10 -5 -13 3.70 3.20 10 5 -12 15.00 4.80 -10 5 12 13.60 3.80 10 5 -12 29.00 6.30 10 -5 -12 14.50 4.40 -10 -5 12 9.50 4.50 -10 5 11 17.70 4.30 10 5 -11 19.50 5.00 10 5 -11 19.90 5.60 -10 -5 11 18.80 5.40 10 -5 -11 30.50 5.00 10 5 -10 23.70 5.60 10 5 -10 27.80 5.70 -10 5 10 19.50 4.20 -10 -5 10 25.20 5.80 10 -5 -10 31.50 5.10 10 5 -9 -0.60 3.40 10 5 -9 0.60 2.30 -10 -5 9 -0.70 3.30 10 -5 -9 2.20 2.30 -10 -5 9 -0.90 2.80 10 5 -8 98.89 8.30 -10 5 8 88.09 7.20 -10 -5 8 78.49 8.70 10 -5 -8 95.39 7.60 -10 -5 8 95.19 8.60 -10 5 7 0.90 2.00 10 5 -7 1.20 2.20 -10 -5 7 6.10 3.60 -10 -5 7 3.30 2.90 10 -5 -7 0.90 1.90 -10 5 6 120.99 8.40 10 5 -6 119.49 8.90 -10 5 6 110.79 8.20 10 -5 -6 114.49 7.80 -10 -5 6 115.89 8.80 -10 -5 6 111.49 9.90 -10 5 5 25.30 4.10 10 5 -5 23.90 4.40 -10 5 5 25.80 3.90 10 -5 -5 32.70 4.40 -10 -5 5 14.50 4.70 -10 -5 5 19.90 4.00 10 5 -4 2.70 2.40 -10 5 4 5.00 1.10 -10 5 4 6.50 2.70 -10 5 4 4.10 1.10 10 5 -4 8.40 2.50 -10 5 4 5.40 2.90 10 -5 -4 2.30 1.90 -10 -5 4 1.90 2.20 -10 -5 4 5.50 2.90 -10 5 3 40.30 4.30 10 5 -3 52.09 5.30 -10 5 3 38.60 5.60 10 5 -3 36.80 5.70 -10 5 3 34.60 3.20 10 -5 -3 40.20 3.80 -10 -5 3 38.90 6.40 -10 -5 3 41.20 4.50 10 5 -2 277.17 12.90 -10 5 2 258.47 12.10 -10 5 2 273.27 12.70 -10 5 2 284.97 12.20 10 5 -2 293.47 14.90 -10 5 2 266.27 14.50 10 -5 -2 290.77 12.40 -10 -5 2 271.57 13.20 -10 -5 2 287.67 16.00 10 5 -1 1.40 2.00 10 5 -1 -0.30 1.60 -10 5 1 2.40 1.90 -10 5 1 2.00 1.70 -10 -5 1 3.50 2.90 -10 -5 1 0.00 2.90 10 -5 -1 -0.10 1.30 -10 5 0 2.20 1.60 -10 5 0 1.10 1.70 10 5 0 -0.80 2.10 -10 5 0 5.80 2.10 -10 5 0 2.60 2.40 10 5 0 1.80 1.60 -10 5 0 3.70 1.50 -10 -5 0 3.50 1.60 -10 -5 0 -2.00 2.60 -10 5 -1 9.90 2.80 10 5 1 8.10 3.40 -10 5 -1 5.50 1.90 -10 5 -1 7.30 1.70 -10 5 -1 7.50 3.20 -10 5 -1 6.60 2.70 -10 -5 -1 8.50 3.30 -10 -5 -1 8.90 1.90 10 5 2 14.70 1.60 -10 5 -2 12.60 2.90 -10 5 -2 10.50 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1 -8 81.79 6.20 11 1 -8 82.79 6.50 -11 1 8 84.89 6.00 11 1 -8 86.19 6.00 -11 1 8 81.59 6.50 -11 -1 8 93.29 7.10 -11 -1 8 92.39 6.60 11 -1 -8 80.59 4.50 -11 -1 8 73.99 5.70 11 -1 -8 83.09 6.10 11 -1 -8 88.09 6.50 11 1 -7 320.97 14.50 -11 1 7 356.46 13.50 11 1 -7 297.87 14.70 -11 1 7 338.77 15.40 -11 1 7 323.27 14.30 11 -1 -7 339.17 12.90 -11 -1 7 323.97 15.20 11 -1 -7 318.17 14.70 -11 -1 7 328.47 15.50 -11 -1 7 337.37 14.60 11 -1 -7 302.27 15.90 11 1 -6 573.74 22.40 11 1 -6 539.35 22.10 -11 1 6 527.75 22.40 11 1 -6 575.14 22.00 -11 1 6 576.14 20.60 -11 1 6 543.95 21.30 -11 -1 6 544.05 21.70 -11 -1 6 520.05 22.50 -11 -1 6 486.25 21.90 11 -1 -6 573.84 20.30 11 -1 -6 531.45 22.10 -11 1 5 31.80 4.30 11 1 -5 24.30 3.40 -11 1 5 26.90 2.80 -11 1 5 20.10 2.30 11 1 -5 24.10 3.50 11 1 -5 26.60 3.70 -11 -1 5 36.40 4.50 11 -1 -5 24.50 3.70 -11 -1 5 28.40 4.00 11 -1 -5 27.50 3.50 11 -1 -5 30.90 2.70 -11 -1 5 28.30 3.00 -11 1 4 364.86 14.70 11 1 -4 374.56 15.70 -11 1 4 358.46 14.60 11 1 -4 392.66 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215.38 10.00 -11 1 0 234.88 10.50 11 1 0 231.58 10.10 11 -1 0 242.08 8.80 11 -1 0 217.38 10.50 11 -1 0 222.48 8.50 -11 -1 0 206.88 10.90 -11 -1 0 221.18 10.20 11 -1 0 229.88 10.90 11 1 1 3.50 1.60 -11 1 -1 4.60 1.90 11 1 1 4.10 1.50 11 1 1 6.00 2.10 11 1 1 3.80 1.40 -11 -1 -1 5.00 1.60 11 -1 1 4.70 2.00 11 -1 1 4.40 0.90 11 -1 1 5.50 0.80 -11 -1 -1 4.30 1.70 11 -1 1 3.20 1.80 -11 1 -2 92.09 6.20 11 1 2 83.09 6.30 11 1 2 85.89 5.10 11 1 2 91.19 5.20 11 1 2 84.39 5.30 -11 1 -2 96.99 6.10 11 -1 2 90.29 6.10 -11 -1 -2 96.19 5.40 11 -1 2 103.99 6.50 11 -1 2 91.19 3.50 -11 -1 -2 95.59 6.50 -11 1 -3 57.19 4.90 11 1 3 49.10 3.80 11 1 3 51.19 3.90 11 1 3 49.99 4.80 11 1 3 50.59 3.70 -11 1 -3 57.99 4.70 -11 -1 -3 62.49 5.00 11 -1 3 52.29 2.10 -11 -1 -3 48.80 3.80 -11 -1 -3 54.89 3.90 11 -1 3 45.40 4.40 11 -1 3 53.39 4.80 11 1 4 231.68 11.80 11 1 4 213.98 10.00 -11 1 -4 206.58 10.60 -11 1 -4 210.08 11.20 11 1 4 214.48 9.70 -11 1 -4 202.48 10.90 -11 -1 -4 231.88 9.90 11 -1 4 202.58 11.30 -11 -1 -4 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55.79 5.40 22 2 -8 54.49 7.90 22 -2 -8 83.19 6.60 -22 -2 8 59.99 8.70 -22 -2 8 65.99 8.50 22 2 -7 113.89 9.70 -22 2 7 122.89 11.30 -22 2 7 130.89 8.40 -22 -2 7 141.49 11.10 22 -2 -7 129.29 8.40 22 2 -6 0.70 3.00 -22 2 6 1.40 2.50 -22 -2 6 -1.20 3.40 22 -2 -6 2.20 4.60 -22 -2 6 -2.40 3.10 22 -2 -6 1.20 2.50 22 2 -5 21.90 5.20 -22 2 5 20.70 4.00 -22 2 5 18.60 4.30 -22 -2 5 24.10 5.20 -22 -2 5 29.00 5.70 22 -2 -5 18.00 3.50 -22 2 4 18.60 5.10 22 2 -4 10.90 4.10 -22 2 4 15.00 3.50 -22 -2 4 14.30 4.70 22 -2 -4 13.10 2.60 22 -2 -4 17.70 4.50 -22 -2 4 14.80 4.50 -22 2 3 19.20 3.80 22 2 -3 13.70 4.20 -22 2 3 10.80 4.50 -22 -2 3 18.00 4.40 22 -2 -3 11.70 2.20 -22 -2 3 15.50 4.30 22 -2 -3 14.20 2.20 -22 2 2 4.40 2.80 22 2 -2 3.10 2.70 -22 2 2 0.80 3.10 -22 -2 2 0.90 3.20 -22 -2 2 5.70 3.50 22 2 -1 24.90 4.70 -22 2 1 36.40 5.50 -22 2 1 24.90 6.00 -22 -2 1 30.60 5.30 -22 -2 1 40.10 7.20 -22 2 0 57.99 6.10 -22 2 0 56.49 8.10 22 2 0 54.99 6.70 -22 -2 0 56.49 7.90 -22 -2 0 56.69 7.00 22 2 1 7.80 2.90 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8.20 -23 -1 3 69.69 8.80 23 1 -2 6.30 3.20 -23 1 2 5.30 3.20 -23 1 2 0.40 3.40 23 -1 -2 4.80 2.20 -23 -1 2 1.90 3.50 -23 -1 2 11.10 4.00 -23 1 1 -2.50 2.80 -23 1 1 -1.50 4.00 23 1 -1 -0.10 2.70 -23 -1 1 7.40 4.20 23 -1 -1 2.60 1.70 -23 -1 1 3.60 3.30 -23 1 0 16.20 4.40 23 1 0 11.90 3.30 -23 1 0 13.10 4.90 -23 -1 0 15.80 5.10 -23 -1 0 21.60 5.20 -23 1 -1 6.70 3.80 23 1 1 -0.50 2.90 -23 1 -1 2.30 3.30 -23 -1 -1 11.40 4.50 -23 -1 -1 2.20 3.80 23 1 2 35.70 4.90 -23 1 -2 42.20 6.80 -23 1 -2 41.30 6.90 -23 -1 -2 37.40 6.90 -23 -1 -2 41.30 6.40 -23 2 6 -3.20 3.50 23 2 -6 2.20 3.70 -23 2 6 4.00 2.70 23 -2 -6 -2.50 2.80 -23 -2 6 2.00 3.70 -23 -2 6 -2.60 3.00 23 2 -5 98.29 9.10 -23 2 5 94.59 7.30 -23 2 5 99.49 9.60 -23 -2 5 103.09 10.20 -23 -2 5 92.89 9.40 23 -2 -5 90.19 6.70 -23 2 4 72.79 9.20 -23 2 4 90.19 7.40 23 2 -4 87.29 8.00 -23 -2 4 50.89 8.10 23 -2 -4 77.59 5.40 -23 -2 4 85.19 8.20 23 2 -3 99.89 8.80 -23 2 3 121.79 8.60 -23 2 3 87.49 9.10 -23 -2 3 90.29 8.90 23 2 -2 6.50 3.10 -23 2 2 5.20 3.60 -23 2 2 7.70 4.00 -23 -2 2 12.80 4.30 -23 2 1 153.88 11.60 23 2 -1 138.49 9.80 -23 -2 1 129.09 11.40 -23 -2 1 140.99 10.40 -24 0 5 0.10 3.00 24 0 -5 0.50 3.40 -24 0 4 28.30 5.90 -24 0 4 39.90 6.50 24 0 -4 29.10 5.00 -24 0 3 -2.70 3.50 24 0 -3 -6.90 2.50 -24 0 3 -1.20 3.30 24 0 -2 0.70 3.30 -24 0 2 -1.80 3.70 -24 0 2 2.70 3.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 39547