Abstract
Fe80Ni20 was prepared by mechanical synthesis using a Fritsch Pulverisette Premium (P7) planetary ball mill at 400 RPM. The alloying process was monitored by measuring the magnetic properties of 14 subsamples taken at different milling times (1-2160 min) as well as structural modifications using powder X-ray diffraction and high-resolution imaging. A macroscopically homogeneous body-centered cubic (bcc) alloy with crystallite sizes below 11 nm and microstrain above 1.2% was reached after 960 min (16 h) of milling. The magnetic properties show three distinct stages: (1) the size reduction of the elementary powders, (2) alloying and (3) reduction in particle size of the final alloy.
| Item Type: | Journal article |
|---|---|
| Faculties: | Geosciences > Department of Earth and Environmental Sciences |
| Subjects: | 500 Science > 550 Earth sciences and geology |
| ISSN: | 0925-8388 |
| Language: | English |
| Item ID: | 67906 |
| Date Deposited: | 19. Jul 2019, 12:23 |
| Last Modified: | 04. Nov 2020, 13:50 |
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