Abstract
A high vacuum oven was constructed to grow LiF single crystals from the vapor phase by the vertical pulling method. Using a special crucible top it is possible to grow oriented single crystals of 23 mm diameter and 70 mm length. At a temperature of about 150 °C above the melting point the maximum pulling rate was found to be 8 mm/h. The purification effect of the sublimation was investigated for Na+-, K+-, Ca++-ions and it was found that the concentration of these impurities is of the order of 10-6, except for sodium for which the purification is much less effective.
Dokumententyp: | Zeitschriftenartikel |
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Fakultät: | Geowissenschaften > Department für Geo- und Umweltwissenschaften > Kristallographie und Materialwissenschaft |
Themengebiete: | 500 Naturwissenschaften und Mathematik > 550 Geowissenschaften, Geologie |
URN: | urn:nbn:de:bvb:19-epub-5589-0 |
Sprache: | Deutsch |
Dokumenten ID: | 5589 |
Datum der Veröffentlichung auf Open Access LMU: | 08. Aug. 2008, 15:36 |
Letzte Änderungen: | 04. Nov. 2020, 12:48 |